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UMATAC Industrial Processes Progress in China Fushun ATP Project Update Colorado School of Mines 34 th Oil Shale Symposium October 14, 2014 UMATAC Industrial Processes ThyssenKrupp Industrial Solutions A company of ThyssenKrupp Industrial


  1. UMATAC Industrial Processes Progress in China – Fushun ATP Project Update Colorado School of Mines 34 th Oil Shale Symposium October 14, 2014 UMATAC Industrial Processes ThyssenKrupp Industrial Solutions A company of ThyssenKrupp Industrial Solutions

  2. UMATAC Industrial Processes Agenda A company of ThyssenKrupp Industrial Solutions Operation Update • Plant is currently producing oil. • 40 day run length achieved. • Oil quality as per design. Fushun Project Background • Mechanical completion in 2010. ATP Plant Main Flare • First oil in 2013. • Continued improvements through 2014. Technical Challenges • Burner fouling. • Flue gas cooler fouling. • Ash system reliability. • New East Open Pit mine. Oil Production Page 2

  3. UMATAC Industrial Processes FMG ATP Plant Flowsheet A company of ThyssenKrupp Industrial Solutions MINE & SPENT ORE ATP COMBUSTION FLUE GAS OIL SHALE DISPOSAL HANDLING PROCESSING AIR SUPPLY CLEAN ‐ UP RECOVERY INERT STOCKPILE BAGHOUSE SCRUBBER FLUE GAS COOLER CYCLONES STACK SHALE INERT SILOS SILOS FUEL OIL COMB. AIR FAN FRACTIONATION ASH SILOS ATP PROCESSOR FEED FLARE FUEL OIL SPENT NAPHTHA RAIL TRANSPORT SHALE SOUR H2O GAS CONTROL UTILITIES & TANK WATER POWER SYSTEM OFFSITES FARM TREATMENT GENERATOR STEAM, PRODUCT ELECTRICITY COOLING WATER LOAD ‐ OUT Page 3

  4. UMATAC Industrial Processes FMG ATP Plant Flowsheet A company of ThyssenKrupp Industrial Solutions ATP MINE & SPENT ORE COMBUSTION FLUE GAS OIL SHALE DISPOSAL HANDLING PROCESSING AIR SUPPLY CLEAN ‐ UP RECOVERY INERT STOCKPILE BAGHOUSE SCRUBBER FLUE GAS COOLER CYCLONES STACK SHALE INERT SILOS SILOS FUEL OIL FUEL GAS COMB. AIR FAN FRACTIONATION ASH SILOS ATP PROCESSOR FEED FLARE FUEL OIL SPENT NAPHTHA RAIL TRANSPORT SHALE SOUR H2O GAS CONTROL TANK WATER POWER UTILITIES & SYSTEM FARM TREATMENT GENERATOR OFFSITES STEAM, PRODUCT ELECTRICITY COOLING WATER LOAD ‐ OUT Page 4

  5. UMATAC Industrial Processes ATP Burner Fouling Update A company of ThyssenKrupp Industrial Solutions ATP Burners • Used vertical retort derived fuel oil from existing FMG plant. • Now using low solids, low water content Slag build-up ATP produced heavy oil, increasing fuel system reliability. Fouling • Determined to be due to exposure of clays to high temperature in flame (slagging). • Proposed solution was to reduce flame intensity. Solution • Automated mechanical cleaning. • Installed Big Blasters ™ (air cannons). • Successful. Page 5

  6. UMATAC Industrial Processes ATP Burner Fouling Update A company of ThyssenKrupp Industrial Solutions ATP Burners • Used vertical retort derived fuel oil from existing FMG plant. • Now using low solids, low water content ATP produced heavy oil, increasing fuel system reliability. Fouling • Determined to be due to exposure of clays to high temperature in flame (slagging). • Proposed solution was to reduce flame Blaster Nozzle intensity. Solution • Automated mechanical cleaning. • Installed Big Blasters ™ (air cannons). • Successful. Page 6

  7. UMATAC Industrial Processes Retrofit ATP to Utilize Off Gas A company of ThyssenKrupp Industrial Solutions ATP Produced Off Gas • Design was to generate 15 MWe of electricity by burning off gas in internal combustion engines. • Generators are not yet commissioned and gas is being flared. Temporary Use • Burn off gas in ATP Processor and displace coke & heavy oil combustion.  Replaced one of three heavy oil burners with a gas burner. Page 7

  8. UMATAC Industrial Processes Flue Gas Cooler / Combustion Air Preheater A company of ThyssenKrupp Industrial Solutions Flue Gas Cooler Cyclones Flue Gas Cooler • Cools flue gas & preheats combustion air. • Ammonia and sulphur dioxide in flue gas. • Process design exit temperature was 175 ° C, reduced to 150 ° C during detail design. Equipment configuration issues • Low tube-wall temperature at cold end. • Low tube-side gas velocity. • Gas distribution. Fouling • Condensation of water and ammonia salts. • Run length initially limited to 7 days, but now exceeding 40 days. Baghouse ATP Processor Page 8

  9. UMATAC Industrial Processes Moisture Condensation & Salt Fouling A company of ThyssenKrupp Industrial Solutions BAGHOUSE HOT FLUE 150 ° C GAS FLUE GAS 335°C COOLER CYCLONES 335 ° C COMB. AIR FAN 35 ° C 265 ° C Tube wall temperatures were below water and ammonia salt condensation temperatures. PREHEATED COOLED COMBUSTION AIR FLUE GAS AIR SUPPLY 265°C 150°C ‐ 35 to +40°C Page 9

  10. UMATAC Industrial Processes Increase Tube Inlet Wall Temperature A company of ThyssenKrupp Industrial Solutions HOT FLUE BAGHOUSE 180 ° C GAS FLUE GAS 335°C CYCLONES COOLER 335 ° C 265 ° C COMB. AIR FAN 80 ° C • Increased combustion air inlet temperature to 80 ° C and reverted to 180 ° C FG exit temp. • Reduced fouling. PREHEATED COOLED COMBUSTION Duct installation AIR FLUE GAS AIR SUPPLY 265°C 180 to 200°C 80°C Page 10

  11. UMATAC Industrial Processes Inlet Air Distribution A company of ThyssenKrupp Industrial Solutions 180 ° C 335 ° C 265 ° C 80 ° C Inlet air distribution resulted in localized over-cooling of tubes. Page 11

  12. UMATAC Industrial Processes Improved Inlet Air Distribution A company of ThyssenKrupp Industrial Solutions 180 ° C 335 ° C 265 ° C 80 ° C Fouling was reduced, and run length increased to over 40 days. Page 12

  13. UMATAC Industrial Processes Ash System Reliability A company of ThyssenKrupp Industrial Solutions Parallel operating/stand-by conveyor belt lines are installed, but both have similar problems. • Complex layout with multiple transfer points. • Transfer point chutes are long, with compound angles and insufficient slope. • Oversized water control valves lead to poor control of ash moistening. Plugged Transfer Chute • Moistened ash is sticky. • Belt skirting is insufficient. • Ash bins bridge and rat-hole. Major modification program has started. Chute modifications Page 13

  14. UMATAC Industrial Processes Oil Shale Feed Variation A company of ThyssenKrupp Industrial Solutions West Pit Mine is Closing • Pilot testing and design were done on West Pit ore: 7% oil yield, 5% free water. • Excellent particulate physical strength. Ash from West Pit Ore East Pit Opened – ore grade during early years of mine operation will be low. • Operations in 2014 mostly used East Pit ore. 4-5% oil, 5-8% water. • Much lower particulate physical strength, resulting in higher fines generation. Ash from East Pit Ore Page 14

  15. UMATAC Industrial Processes Oil Shale Feed Variation A company of ThyssenKrupp Industrial Solutions West Pit Mine is Closing • Pilot testing and design were done on West Pit ore: 7% oil yield, 5% free water. • Excellent particulate physical strength. Ash from West Pit Ore East Pit Opened – ore grade during early years of mine operation will be low. • Operations in 2014 mostly used East Pit ore. 4-5% oil, 5-8% water. • Much lower particulate physical strength, resulting in higher fines generation. Ash from East Pit Ore Overburden Green Shale Oil Shale Coal Page 15

  16. UMATAC Industrial Processes 2014 Operations A company of ThyssenKrupp Industrial Solutions FMG is taking a cautious but firm approach to operation in 2014. This year’s targets were to achieve a 30 day run (done) and then a 90 day run. FMG has added a second 30 day run to test reliability improvements. Oil shale throughput is 70 to 80% of design. May 2014 Oil Shale and Ash Trains Page 16

  17. UMATAC Industrial Processes 2014 Operations A company of ThyssenKrupp Industrial Solutions Start Date Run Length Feed Rate Notes (days) Jan. 2014 7 Inert feed Baghouse bag replacement. 15 April 2014 Inert feed Check-out run, refractory dry-out. Oil Shale FG cooler modifications, ash system 15 May 2014 140-170 t/h improvements, Big Blaster installation. Oil Shale Successful improvement of plant July 2014 40 160-180 t/h operability. (70-80% of design) Currently in Oil Shale Targeting 30 day run, to be followed by Oct. 2014 Operation 160-180 t/h 90 day operation. July 2014 Page 17

  18. UMATAC Industrial Processes FMG ATP Processor Operating Hours A company of ThyssenKrupp Industrial Solutions First oil Mechanical completion ~ 200,000 tonnes oil shale processed, 70,000 bbls oil produced to date in 2014. Page 18

  19. UMATAC Industrial Processes Oil Shale Operation July 2014 A company of ThyssenKrupp Industrial Solutions Page 19

  20. UMATAC Industrial Processes Oil Shale Operation July 2014 A company of ThyssenKrupp Industrial Solutions Temperature Control Feed & Ash System Upsets Page 20

  21. UMATAC Industrial Processes ATP Operations Video A company of ThyssenKrupp Industrial Solutions 2014 Video – ATP Commercial Oil Shale Operations (China) View online at UMATAC Industrial Processes Videos http://youtu.be/XxNLuK6DLuE Page 21

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