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Magnetometry standard for the muon g2 experiment g2 p measurement - - PowerPoint PPT Presentation

Magnetometry standard for the muon g2 experiment g2 p measurement NMR magnetometers Absolute calibration problem 3 He magnetometry How to polarize 3 He state of the art Sam Henry, University of Oxford 1 The g2


slide-1
SLIDE 1

Magnetometry standard for the muon g−2 experiment

  • g−2 ωp measurement
  • NMR magnetometers
  • Absolute calibration problem
  • 3He magnetometry
  • How to polarize 3He – state of the art

Sam Henry, University of Oxford

1

slide-2
SLIDE 2

The g−2 magnetic field measurement

2

eB m a

a

  

We need to measure the magnitude of the 1.45T field to 0.07ppm…

p a p p a

a      

 

 

Measure magnetic field in terms of proton precession frequency

(Measured by E1054 muonium experiment)

Measure with proton NMR magnetometer probes …averaged over muon distribution (7m radius ring)

  • 378 fixed probes – monitor

field when beam is on

  • 17 mobile trolley probes –

map field when beam is off

slide-3
SLIDE 3

3

Pulsed Nuclear Magnetic Resonance Magnetometry

Free Induction Decay NMR of proton in water sample

  • Apply 61.74MHz pulse to Ls coil to rotate polarization of

protons by π/2 to magnetic field

  • Spins precess at ωp – rotating dipoles produce magnetic signal

– measure emf in Lp coil

  • Digitize – analyse signal to determine frequency  61.79MHz
slide-4
SLIDE 4

4

Absolute Calibration Problem

  • ωp is a measure of the absolute magnitude of the magnetic field
  • But some absolutes are more absolute than others
  • Every probe will introduce shift ~0.1ppm due to paramagnetic

properties of probe material

  • All probes calibrated against standard probe with spherical water

sample

 B

1 B

t p

  

 

6 p p O H

10 15 689 , 25 1

2

               

Protons in spherical water sample Free protons

Philips et al. Metrologia 1977, 13, 179-195

  • 50ppb accuracy

for Brookhaven experiment

  • Target 35ppb for

Fermilab

s p b O H t

2

        

slide-5
SLIDE 5

Measurement of λ=μμ/μp (E1054 experiment)

  • Used same standard magnetometer probe
  • W. Liu et al., PRL 82 711 (1999)
  • High precision measurements of Zeeman hyperfine transitions in

muonium (μ+e‒)

 

37 18334524 3.

p

  

120ppb

  • QED theory, using mμ/me set by hyperfine interval measurement

 

84 183345107 3.

p

  

26ppb

5

Limited by 14ppb measurement by Philips et al to take proton in water to free proton

slide-6
SLIDE 6

6

Proposed 3He Absolute Calibration Probe

     

 

6 O H

10 C 7 . 34 T 30 01036 . 14 792 . 25

2

      

 

6 He

10 10 43 967 . 59

3

  

  • Lower uncertainty on diamagnetic shielding
  • Temperature coefficient 100 times smaller
  • Negligible magnetic susceptibility – no sample shape dependence
  • NMR signal per atom larger – potential to use smaller probe

Challenge:

  • Polarise sufficient amount of 3He to get useful NMR signal
slide-7
SLIDE 7

Polarisation of 3He for NMR

7

  • Cryogenic techniques
  • ‘Brute force’ approach
  • Gas at 4.2K in static field
  • Optical pumping
  • Spin Exchange (SEOP) – mixture of 3He and other atoms (e.g. K)
  • High pressure, long time needed
  • Metastability Exchange (MEOP)
  • Low pressure gas (~1mbar)
  • 1083nm semiconductor laser diode
  • Significant improvements in recent years to allow use in

large fields at higher pressures

slide-8
SLIDE 8

3He magnetometry – work at NPL

  • Development of optical

pumping techniques at NPL in 1990s to measure fields of 0.6T With spherical water sample measured to 4.3×10-9 Compare to ESR frequency of atomic hydrogen

  • Use as reference NMR

frequency in physical chemistry research

 

p h

He  

3

 

B h

He  

3

8

slide-9
SLIDE 9

9

Polarized 3He work for medical applications

  • Recent development

allow larger polarizations for larger pressures

slide-10
SLIDE 10

10

3He magnetometry for g−2 This project:

  • Cross-check calibration of standard spherical water probe
  • Probes should agree to within 4.2ppb

Longer term?

  • Replacement for standard water probe?
  • Could reduce uncertainty on calibration to 14ppb (proton in

water – free proton)

  • Use 3He in plunging probes
  • Replace free proton with helion as magnetic field reference?
  • Need precision measurement of μμ/μ3He
slide-11
SLIDE 11

11

Conclusions

  • g−2 experiment requires monitoring of magnetic field in muon ring

to 0.07ppm

  • Proton NMR magnetometers
  • 378 fixed + 17 trolley probes calibrated against standard probe
  • Spherical water probe: limited by shape and temperature

dependent shifts

  • 3He probe: potential to significantly improve accuracy and will

provide independent check

  • Challenge: polarise large number of 3He nuclei in 1.45T field