Future Installations-ILL R. Cubitt APEX- Instrument for Industry - - PowerPoint PPT Presentation

future installations ill r cubitt apex instrument for
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Future Installations-ILL R. Cubitt APEX- Instrument for Industry - - PowerPoint PPT Presentation

Future Installations-ILL R. Cubitt APEX- Instrument for Industry Design Options D33-Reusing a SANS instrument for imaging Neutrograph All Purpose EXperiments- APEX GOAL: To build an instrument that has the widest possible range of


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Future Installations-ILL

  • R. Cubitt

APEX- Instrument for Industry Design Options D33-Reusing a SANS instrument for imaging Neutrograph

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SLIDE 2

GOAL: To build an instrument that has the widest possible range

  • f industrial applications for the least money without compromising any
  • ption

Reflectometry (RAINBOWS) q=0.005-0.3 20x D17 at mid range q Very efficient method to produce high performance reflectometry at low cost SANS q=0.001-0.5 same as D33 (7mm samples) Well known that SANS can be scaled down without loss of performance Tomography R=10 microns-1 mm best in world flux/resolution Dewhurst has pointed out that SANS and Tomography requirements are the same All Purpose EXperiments- APEX

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SLIDE 3

D1=5m prism

a

L sample D2=5m

Uses refractive optics to measure wavelength Gain~5x D17 over first angle Q=0.01-0.1 Might be a case to combine with radiography or thin absorbing samples Reflectometry Option-RAINBOWS

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SANS Option

sample selector detector

Collimation length fixed at 5m- with variable source size can match D33 D33 source 30x30 mm^2 coll=12.8,10.3,7.8,5.3, 2.8 60x60 @ 5m (D33 coll=2.5m) 15x15 @ 5m (D33 coll=10m) Det 200x200 mm^2 Qmax=0.5A @ det=200 mm Qmin=0.003 @ 5m 6A (0.001 @ 18A) Combine with radiography with large distance for scattering contrast

0.2-5m 5m

Source 60x60 30x30 15x15 Schillinger

  • Et. al. FRMII
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Tomography Option

sample selector

Variable wavelength+white option M=2 beam total size=200x200 @ 6A & 5m Good range of resolution 10 microns to 1 mm Lead box 15 cm thick including roof is required. Keep Neutrograph in reactor low res high flux Wish list:

  • 1. cold neutrons preferred ✔
  • 2. high intensity ✔ ✔
  • 3. high collimation (res=10 microns) ✔
  • 4. options for energy selection ✔
  • 5. polarization options- D33
  • 6. highest spatial resolution ✔

D1=5m

Source D2 Res mm 60x60 8cm 1000 60x60 1cm 125 5x5 8 cm 80 5x5 1 cm 10

D2 Res=(D2/D1)*S S

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End H521 Monitor

Source aperture: translation range360 deg 0.1 deg 10 positions: 3 for reflectometry (1x120, 2x120,3x120) 7 for sans/tomo: (60,50,40,30,20,10,5 diameter) each position take up 70 mm

Source aperture 2x Fast shutter

in/out air piston:

Selector

Selector translation with manual rotation to 6% resolution position Translation must cover sel/out/mono option so 700 mm range 0.1mm precision

Graphite

5-meters long Starts at 60x120 finishes 200x200 He3 filled- no vacuum

collimation box B4C absorbing baffles

Large frames for tomo option from 200x200 down to 10x70mm manual changing

  • Max. weight 50 kg

height drive range 500mm precision 0,1 mm x-translation range 500 mm precision 10 microns rotation: 360 deg; 0.005 deg precision gonio ±3 deg 0.005 deg precision Use old sans stack?

Sample stack

Reflectometry slits X 10mm-50 micron prec=10 micron Slits Y 70mm-5mm prec 0.1mm+

Source Aperture Reflectometry

Components before sample

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SLIDE 7

Components after sample

Sample stack Detector He filled tank

~350mm diameter 5.5 m long rotation -1-5deg precision 0.005 deg Tank translation 500mm precision 0.1 mm Detector translation inside tank range=5m precision 0.1mm

Detector

200x200 - 4000x4000 pixel variable focal area ccd scintilator prism movements for max weight 500g translation range 10 mm precision 10 microns rotation range 10 deg precision 0.005 deg gonio range ± 2 deg precision 0.005 deg

Detector He filled tank

~350mm diameter 5.5 m long rotation -1-5deg precision 0.005 deg Tank translation 500mm precision 0.1 mm Detector translation inside tank range=5m precision 0.1mm

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Preliminary Design- Benjamin Giroud ILL22 after ADAM

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SLIDE 9

9

Depolarization Radiography of thin steel Depolarization Transmission Magnetized section He3 Object Polarised beam

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Source 0.5mmØ Image

 Magnification ~ x6 → x16  Spatial resolution ~0.9 → 0.5mm  Absorption & Scattering Contrast  Wavelength selectivity

Object

D33

SANS Detector: 64cm x 64cm 2.5 x 5mm resolution

Using the SANS instrument D33 for Imaging- Charles Dewhurst

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Conclusions APEX, D33 and the Neutrograph have new life breathed into them Benjamin Giroud Duncan Atkins Jaime Segura-Ruiz Charles Dewhurst Thilo Perling Jerome Beaucour