Status of the q n Experiment in Mainz C. Siemensen Institute of - - PowerPoint PPT Presentation

status of the q n experiment in mainz
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Status of the q n Experiment in Mainz C. Siemensen Institute of - - PowerPoint PPT Presentation

Status of the q n Experiment in Mainz C. Siemensen Institute of Nuclear Chemistry Johannes Gutenberg-University of Mainz International UCN Workshop Mainz, Germany, April 11 th -15 th, 2016 April 13th, 2016 C. Siemensen (Kernchemie) Status of


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SLIDE 1

Status of the qn Experiment in Mainz

  • C. Siemensen

Institute of Nuclear Chemistry Johannes Gutenberg-University of Mainz International UCN Workshop Mainz, Germany, April 11 th -15 th, 2016

April 13th, 2016

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 1 / 22

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SLIDE 2

ε /qn in the Past

1

ε /qn in the Past

2

Apparatus

3

Fomblin as Horizontal Mirror

4

Charge Measurement

5

Summary and Outlook

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 2 / 22

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SLIDE 3

ε /qn in the Past

Determination of ε:

Charge of the free neutron using UCN "former experiment" Scattering myon neutrinos - electrons Neutrinos of supernova SN1987A Neutral matter ~HV (Borisov) Charge of the free neutron using CN (Baumann)

1

1https://www.cfa.harvard.edu/sins/datajan2007/sn1987a_wide.tif

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 3 / 22

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SLIDE 4

Apparatus

1

ε /qn in the Past

2

Apparatus

3

Fomblin as Horizontal Mirror

4

Charge Measurement

5

Summary and Outlook

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 4 / 22

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SLIDE 5

Apparatus

Principle of Measurement

UCN beam

  • ptical axis

cylindrical mirror input grating unpertubed beam deflected beam force detector exit grating +

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 5 / 22

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SLIDE 6

Apparatus

Principle of Measurement

UCN beam

  • ptical axis

cylindrical mirror input grating unpertubed beam deflected beam force detector exit grating +

  • detector

gratings electrodes cylindrical mirror former experiment

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 5 / 22

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SLIDE 7

Apparatus

Setup

cylindrical mirror electrode Fomblin basin exit gratings input grating

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 6 / 22

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SLIDE 8

Apparatus

Reduction of the Number of Horizontal Reflections

former experiment* new geometry

entrance guide

  • cyl. mirror

detector & grating

0.001 0.01 0.1 1 5 10 15 20 25 30 35 40 45 UCN number of hor. reflections former exp. 1m former exp.* 1.5m new geometry 1.5m

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 7 / 22

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SLIDE 9

Apparatus

Reduction of the Number of Horizontal Reflections

former experiment* new geometry

entrance guide

  • cyl. mirror

detector & grating

0.001 0.01 0.1 1 5 10 15 20 25 30 35 40 45 UCN number of hor. reflections former exp. 1m former exp.* 1.5m new geometry 1.5m

Mean reflections: former exp. 1.0m : ¯ R ≈ 21.7 former exp.* 1.5m : ¯ R ≈ 31.9 new geometry 1.5m : ¯ R ≈ 1.7

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 7 / 22

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SLIDE 10

Apparatus

Automatic Adjustment System

gratings: ∆α ≤ 90µrad mirror:∆α ≤ 350µrad

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 8 / 22

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SLIDE 11

Apparatus

Electrode System

Without conditioning and cleanroom conditions: Emax ≈ 1.6 MV

m were

possible

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 9 / 22

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SLIDE 12

Fomblin as Horizontal Mirror

1

ε /qn in the Past

2

Apparatus

3

Fomblin as Horizontal Mirror

4

Charge Measurement

5

Summary and Outlook

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 10 / 22

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SLIDE 13

Fomblin as Horizontal Mirror

Fomblin Y-HVAC 140/13

pros high viscosity: 1508cSt2 dielectric constant independent from electric field (up to 640kV/m) surface roughness ≈ 5.24Å cons no solubility in most detergents dissolved air bubbles pop under vacuum dielectric (moves if ∇ E = 0) cracks when freezed out

2Solvay Solexis. Perfluorpolyether - Fomblin Y, M und Z-Öle + Fomblin Fette. 2004

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 11 / 22

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SLIDE 14

Fomblin as Horizontal Mirror

Fomblin as Horizontal Mirror

  • 0.04
  • 0.02

0.02 0.04 0.06

  • 50
  • 40
  • 30
  • 20
  • 10

residuals Δε T / °C 20kV/m 200kV/m 404kV/m 579kV/m 640kV/m

1 e− 4 1 e− 3 1 e− 2 1 e− 1 1 e0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 R/Rf q2[1/Å ]

2

ambient temperature Fit 0°C Fit − 30°C Fit − 55°C Fit

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 12 / 22

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SLIDE 15

Fomblin as Horizontal Mirror

Summary

new geometry ⇒ reduction of the number of horizontal reflections prolongated flight path ⇒ doubling of the sensitivity automatic adjustment system ⇒ smaller slit widths improved electrode system ⇒ higher HV-stability liquid Fomblin mirror ⇒ no adjustment required

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 13 / 22

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SLIDE 16

Fomblin as Horizontal Mirror

Summary

new geometry ⇒ reduction of the number of horizontal reflections prolongated flight path ⇒ doubling of the sensitivity automatic adjustment system ⇒ smaller slit widths improved electrode system ⇒ higher HV-stability liquid Fomblin mirror ⇒ no adjustment required

⇒ δqn ≈ 1.3· 10−21 e √ d

level of Baumann obtainable within one day

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 13 / 22

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SLIDE 17

Charge Measurement

1

ε /qn in the Past

2

Apparatus

3

Fomblin as Horizontal Mirror

4

Charge Measurement

5

Summary and Outlook

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 14 / 22

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SLIDE 18

Charge Measurement

Charge Measurement

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 15 / 22

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SLIDE 19

Charge Measurement

Parameters of the Experiment

Beam time 3.11. - 1.12.2014 at UCN, ILL: Parameters: Value: mean flight path t in E-field E

(0.70± 0.20)s

neutron fluxes n1 ≈ 19 1

s n2 ≈ 53 1 s n3 ≈ 57 1 s n4 ≈ 40 1 s

electric field ∆E 1.2MV

m

gratings 0.4mm slit, 0.7mm spacing slopes

∂xn1 = −6273 1

s·m ∂xn2 = −37173 1 s·m

∂xn3 = 45820 1

s·m ∂xn4 = 44563 1 s·m

  • verall measurement time

τ = 3.44· 105 s (approx 4 days)

statistical sensitivity 2.4· 10−20

e

√ d (3.8 times larger)

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 16 / 22

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SLIDE 20

Charge Measurement

Modulations of the Count Rate

20 30 40 50 60 70 80 6 7 8 9 10 11 12 13 14 15 count rate / 1/s x / mm APO APU Det 1 Det 2 Det 3 Det 4

1 2 3 4

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 17 / 22

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SLIDE 21

Charge Measurement

Results

20 40 60 80 100 120 140

  • 200-150-100 -50

50 100 150 200 frequency Δx / µm Det 1 Det 2 Det 3 Det 4

∆x1 = (7.19± 2.58)· 10−6 m ∆x2 = (5.34± 0.69)· 10−6 m ∆x3 = (3.35± 0.60)· 10−6 m ∆x4 = (4.01± 0.52)· 10−6 m

10 20 30 40 50 60 70 80 90

  • 3e-18-2e-18-1e-18

1e-18 2e-18 3e-18 frequency charge qn/e

qn =(−1.82± 0.24stat. ± 0.09∂xn ...

...± 0.02E ± 0.78t)· 10−19e

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 18 / 22

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SLIDE 22

Charge Measurement

Results - Discussion

charge of the free neutron (Baumann, 1987): |ε| ≤ 10−21 e

Possible systematic effects: motion of the HV-switch breakdown of the fields

  • ptics in E-field

Fomblin in E-field

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 19 / 22

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SLIDE 23

Charge Measurement

Results - Discussion

charge of the free neutron (Baumann, 1987): |ε| ≤ 10−21 e

Possible systematic effects: motion of the HV-switch breakdown of the fields

  • ptics in E−field ? ⇒ n ↔ γ in E-field: ∆xγ ≈ 1.8µm

Fomblin in E−field ? ⇒ distortion by

  • U+

−|U−| ≈ 5.2kV

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 19 / 22

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SLIDE 24

Charge Measurement

Results - Discussion

charge of the free neutron (Baumann, 1987): |ε| ≤ 10−21 e

Possible systematic effects: motion of the HV-switch breakdown of the fields

  • ptics in E−field ? ⇒ n ↔ γ in E-field: ∆xγ ≈ 1.8µm

Fomblin in E−field ? ⇒ distortion by

  • U+

−|U−| ≈ 5.2kV

considering both effects: qn =(−0.32± 1.22stat. ± 0.39∂xn ±...

...± 0.10E ± 0.14t ± 1.29xkorr.)· 10−20e ⇒ qn ≤ 1.8· 10−20 e

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 19 / 22

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SLIDE 25

Charge Measurement

Effective Tilt of the Horizontal Mirror

0.1 0.2 0.3 0.4 0.5

  • 4
  • 2

2 4 surface distortion / µm x / cm symmetric asymmetric 2,5kV asymmetric 5,0kV asymmetric 10kV

Basin Shielding Electrodes

δeff =

1 xr − xl

xr

  • xl

dSF(x) dx ˜ Ω(x)dx δeff(symm.) = −0.04µrad δeff(asymm.2.5kV) = −0.37µrad δeff(asymm.5.0kV) = −0.73µrad δeff(asymm.10kV) = −1.28µrad

∆F = ∆E · qn = g mn sinδα ⇒ δα ≈ 1.5µrad ⇒ ∆U± ≈ 5.2kV

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 20 / 22

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SLIDE 26

Summary and Outlook

1

ε /qn in the Past

2

Apparatus

3

Fomblin as Horizontal Mirror

4

Charge Measurement

5

Summary and Outlook

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 21 / 22

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SLIDE 27

Summary and Outlook

Summary and Outlook

charge of the free neutron linked to the problem of ECQ drafting a new charge experiment (dedicated geometry, new HV-system, adjustment, . . . ) first charge experiment since 1987: 2.4· 10−20

e

√ d

understanding of systematic effects: replace horizontal mirror/ extended screening, assure electric potential of the electrodes potentially δqn ≈ 1.3· 10−21

e

√ d in the near future

  • C. Siemensen (Kernchemie)

Status of the qn Experiment in Mainz April 13th, 2016 22 / 22