NFPA 2112 Round Robin Manikin Testing NFPA 2112 Thermal Manikin Task - - PowerPoint PPT Presentation
NFPA 2112 Round Robin Manikin Testing NFPA 2112 Thermal Manikin Task - - PowerPoint PPT Presentation
NFPA 2112 Round Robin Manikin Testing NFPA 2112 Thermal Manikin Task Group April 29 th , 2016 Issue In recent years the burn injury predictions have started to differ significantly more than in the past Test Results for 4.5 oz (154 g/m2) Nomex
Issue
- In recent years the burn injury predictions
have started to differ significantly more than in the past
Test Results for 4.5 oz (154 g/m2) Nomex III A with underwear
Test Method ASTM F1930 -11 Results from Alberta (TPBI) 40.8 % Results from DuPont (TPBI) 20 % Results from NCSU (TPBI) 37 %
NFPA 2112 Task Group Request
- Using the same fabrics and test procedure
– Determine the expected differences between laboratories performing NFPA 2112 testing
- Propose language that might improve
agreement between labs
Task Group Language Proposed to NFPA 2112
– 3 second nude calibration exposure
- Average incident heat flux calculated from one to three
seconds
- Numerical fitting function not to be used to calculate
incident heat flux
- Average incident heat flux is greater than or equal to 79
kw/m2 at 1 second mark
– In situ testing at 4, 8, and 12kW/m2
- 6 sensors to be verified (right and left arms and legs, chest
and back)
- 4, 8, and 12kW/m2 levels
2011 ISO Round Robin Data
ISO 13506 Results Section 9.5.3 120 s data acquisition
10 20 30 40 50 60 70 1 2 3 4 5 6 7
Laboratory Percent Under Garment Second Degree or Worse
NFPA 2112 Round Robin Testing 2015
– Six fabrics tested
- Fabric A: 4.5 osy Aramid
- Fabric B: 5.8 osy FR Modacrylic/Aramid
- Fabric C: 3.4 osy Aramid
- Fabric D: 6.0 osy Aramid
- Fabric E: 7.5 osy FR Cotton
- Fabric F: 6.5 osy FR Cotton blend
– Three Second Exposure, with 100% cotton t‐shirt and briefs
Round Robin Results
– Five Labs Participated
- University of Alberta
- DuPont Richmond
- North Carolina State University
- Aitex
- BTTG
– Results Anonymized for the five labs
- Labs 3 and 4 compliant with proposed task group language
- Labs 1, 2, and 5 not compliant with proposed task group
language
Round Robin Results‐Analysis
– Display Results – Identify any outliers – Compare labs results vs. fabric types – Can each lab distinguish between fabric types
Round Robin Results‐All Labs
10 20 30 40 50 60 70
4.5 osy Aramid 5.8 osy FR Modacrylic/Aramid 3.4 osy Aramid 6.0 osy Aramid 7.5 osy FR Cotton 6.5 osy FR Cotton Blend
Overall % Body Burn
ALL LABS AVERAGE BURN INJURY PREDICTIONS
Lab #1 Lab 2 Lab 3 Lab 4 Lab 5
Test Method ASTM F1930- 00 ASTM F1930 -11 Skin thicknesses μm 50/1500/10000 (based on whole body) 75/1125/3885 (based on forearm) Results from Alberta (TPBI) 47.2 % 40.8 % Results from DuPont (TPBI) 36 % 20 % Results from NCSU (TPBI) 41 % 37 % reduction in reported value Alberta: 6.4 % reduction in reported value DuPont: 16 % reduction in reported value NCSU: 4 %
Test Results for 4.5 oz (154 g/m2) Nomex III A with underwear using different skin properties, 3 sec. exposure at 84 kW/m2. Percent 2nd degree or worse, including head.
* Slide from “ASTM New Orleans LA, January 1st, 2015” Presentation by Douglas Dale, University of Alberta
Lab Results Results for Fabric A‐(4.5 osy Aramid)
95% Confidence Interval Prediction Mean‐36.62% Lower‐95% Upper‐95% 33.77% 39.46%
Lab Results (1‐4) for Fabric A (4.5 osy Aramid)
Lab Lab p‐Value 4 1 0.0279* 4 2 0.0787 3 1 0.1038 3 2 0.2670 4 3 0.6520 2 1 0.9833
Lab Results Results for Fabric B‐(5.8osy Modacrylic/Aramid)
95% Confidence Interval Prediction Mean‐19.70% Lower‐95% Upper‐95% 14.68% 24.73%
Lab Results (1‐4) for Fabric B (5.8osy Modacrylic/Aramid)
Lab Lab p‐Value 3 2 <.0001* 4 2 0.0001* 3 1 0.0027* 4 1 0.0095* 1 2 0.0740 3 4 0.9404
95% Confidence Interval Prediction Mean‐48.79% Lower‐95% Upper‐95% 47.76% 49.82%
Lab Results (1‐4) for Fabric C (3.4osy Aramid)
Lab Lab p‐Value 4 2 0.0181* 3 2 0.0840 1 2 0.2876 4 1 0.3798 4 3 0.6567 3 1 0.9203
Lab Results Results for Fabric C‐(3.4osy Aramid)
Lab Results (1‐4) Results for Fabric D‐(6.0osy Aramid)
95% Confidence Interval Prediction Mean‐19.51% Lower‐95% Upper‐95% 15.24% 23.77%
Lab Results (1‐4) for Fabric D (6.0osy Aramid)
Lab Lab p‐Value 4 1 <.0001* 4 2 <.0001* 4 3 0.0002* 3 1 0.0019* 3 2 0.0064* 2 1 0.7342
Lab Results (1‐4) Results for Fabric E‐(7.5osy FR Cotton)
95% Confidence Interval Prediction Mean‐27.56% Lower‐95% Upper‐95% 20.85% 34.07%
Lab Results (1‐4) Results for Fabric E‐(7.5osy FR Cotton)
Lab Lab p‐Value 2 1 0.0037* 4 1 0.0061* 3 1 0.1158 2 3 0.1212 4 3 0.2116 2 4 0.9759
Lab Results (1‐4) Results for Fabric F‐(6.5osy FR Cotton Blend)
95% Confidence Interval Prediction Mean‐30.80% Lower‐95% Upper‐95% 23.30% 38.31%
Lab Results (1‐4) Results for Fabric F‐(6.5osy FR Cotton Blend)
Lab Lab p‐Value 4 1 0.0003* 2 1 0.0012* 3 1 0.0105* 4 3 0.0613 2 3 0.3437 4 2 0.6058
Can a Lab Distinguish Between the Fabrics?
Can a Lab Distinguish Between the Fabrics?
Lab 1 Lab 2 Lab 3 Lab 4 Lab 5
Historical Perspective North American Labs
ASTM 2002 vs. NFPA 2112‐2015 Round Robin
95% Confidence Interval Prediction Mean: 11.37% Lower‐95% Upper‐95% 9.41% 13.33%
North American Labs: ASTM F1930‐2002 Round Robin Results 3 second exposure, no underwear
95% Confidence Interval Prediction Mean: 28.03 Lower‐95% Upper‐95% 20.53% 35.54% 95% Confidence Interval Prediction Mean: 35.62 Lower‐95% Upper‐95% 28.46% 42.78% FR Cotton, 9 osy Aramid, 6 osy PBI/Kevlar, 4.5 osy
Lab Lab p‐Value K P 0.0178* N P 0.1036 K N 0.3741 Lab Lab p‐Value K P 0.0086* K N 0.0249* N P 0.6219 Lab Lab p‐Value K P 0.0021* K N 0.0033* N P 0.8560
North American Labs: NFPA 2112‐2015 Round Robin Results 3 second exposure, with underwear
Fabric A: 4.5 osy Aramid Fabric B: FR Modacrylic/Aramid Fabric C: 3.4 osy Aramid
95% Confidence Interval Prediction Mean: 38.08% Lower‐95% Upper‐95% 35.69% 40.46% 95% Confidence Interval Prediction Mean: 20.72 Lower‐95% Upper‐95% 14.37% 27.07% 95% Confidence Interval Prediction Mean: 48.8 Lower‐95% Upper‐95% 47.45% 50.14%
Lab Lab p‐Value 4 2 <.0001* 3 2 0.0007* 4 3 0.0103* Lab Lab p‐Value 3 2 <.0001* 4 2 <.0001* 3 4 0.7954 Lab Lab p‐Value 4 2 0.0207* 3 2 0.0778 4 3 0.5420
North American Labs: NFPA 2112‐2015 Round Robin Results 3 second exposure, with underwear
Fabric D: 6.0 osy Aramid Fabric E: 7.5 osy FR Cotton Fabric F: 6.5 osy FR Cotton Blend
95% Confidence Interval Prediction Mean: 21.5% Lower‐95% Upper‐95% 16.46% 26.56% 95% Confidence Interval Prediction Mean: 32.01% Lower‐95% Upper‐95% 26.28% 37.74% 95% Confidence Interval Prediction Mean: 36.47% Lower‐95% Upper‐95% 31.25% 41.69%
Lab Lab p‐Value 4 2 <.0001* 4 3 0.0002* 3 2 0.0040* Lab Lab p‐Value 2 3 0.1442 4 3 0.2250 2 4 0.9348 Lab Lab p‐Value 4 3 0.0773 2 3 0.3189 4 2 0.5336