anti-Bromination of alkenes: direct bromonium ion intermediate - - PowerPoint PPT Presentation

anti bromination of alkenes direct bromonium ion
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anti-Bromination of alkenes: direct bromonium ion intermediate - - PowerPoint PPT Presentation

anti-Bromination of alkenes: direct bromonium ion intermediate formation C + C Br Br Br Br C .. C + Br C C C + Br Br Br- Br C C C Br Orbital interactions in the anti-Bromination of alkenes: direct


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SLIDE 1

anti-Bromination of alkenes: direct bromonium ion intermediate formation

C C Br Br C C Br Br C C Br Br C C Br C C Br Br δ+ δ− + Br- .. δ+ δ−

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SLIDE 2

Orbital interactions in the anti-Bromination of alkenes: direct bromonium ion intermediate formation

C C Br Br C C Br Br C C Br Br C C Br C C Br Br δ+ δ− + Br-

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SLIDE 3

Alkyl substituents on the bromomium ion desymmetrize it: the more substitued carbon can bear more

  • f the burden of the bromine’s positive charge:

So, the electrophilic Br ends up on the less substituted carbon and the nucleophilic Br ends up on the more substituted carbon.

C C H H Br Br C C H H Br Br C C H H Br Br C C Br H H C C H H Br Br δ+ δ− Br- .. δ+ δ− δ+ δ+

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SLIDE 4

This is a Markovnikov-like addition: when adding HCl, the electrophile (H) ends up on the less substituted carbon and the nucleophile (Cl) ends up on the more substituted carbon. Although the mechanism is different, the regiochemistry is not: C C H H H Cl C C H H H C C H H H Cl Cl- δ+ δ− +

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SLIDE 5

H H H Cl H Cl Cl H Cl H H H Cl Cl Cl H Cl H H Cl Cl H Cl H H Cl Cl2 CH2Cl2 H H H H Cl Cl Cl H Cl H Cl H Cl H H Cl H Cl Cl2 CH2Cl2

Anti-addition of Cl2 to trans-3-hexene meso Anti-addition of Cl2 to cis-3-hexene enantiomers

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SLIDE 6

R H H H R O H O H H

  • 1. O3
  • 2. Zn, H2O

+ R H R

2

H R O H O R

2

H

  • 1. O3
  • 2. Zn, H2O

+ R R

1

H H R O R

1

O H H

  • 1. O3
  • 2. Zn, H2O

+ R R

1

R

2

H R O R

1

O R

2

H

  • 1. O3
  • 2. Zn, H2O

+ R R

1

R

2

R

3

R O R

1

O R

2

R

3

  • 1. O3
  • 2. Zn, H2O

+

Ozonolysis of alkenes

aldehyde ketone mono formaldehyde ketone tri aldehyde terminal di formaldehyde ketone aldehyde tetra ketone internal di (E) or (Z) aldehyde

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SLIDE 7

H O H H O

  • 1. O3
  • 2. Zn, H2O

It doesn’t matter if the alkene is a cycloalkene:

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SLIDE 8

Addition reactions of carbon-carbon double bonds Reaction Adds Regiochemistry Diastereoselective? Rearrangement observed? Hydrohalogenation H–X Markovnikov No Yes H–Br AntiMarkovnikov No No Hydration Acid-catalyzed Hydration H–OH Markonikov No Yes Oxymercuration- demercuration H–OH Markovnikov No No Borohydration-

  • xidation

H–OH AntiMarkovnikov Yes - syn No Hydrogenation H–H

  • Yes - syn

No * Halogenation X–X

  • Yes - anti

No Halohydroxylation X–OH Markovnikov Yes - anti No Dihydroxylation Epoxidation- acid hydroylsis HO–OH

  • Yes - anti

No * OsO4 HO–OH

  • Yes - syn

No Oxidative cleavage O + O

  • No

No