spICP-MS – tier 1 method
“People behind the experiments”
Anna Katarzyna Undas (RIKILT)
NanoDefine Outreach Event
Brussels, September 2017
NanoDefine is funded by the European Community's Seventh Framework Programme under Grant Agreement-604347
spICP-MS tier 1 method People behind the experiments Anna - - PowerPoint PPT Presentation
spICP-MS tier 1 method People behind the experiments Anna Katarzyna Undas (RIKILT) NanoDefine Outreach Event Brussels, September 2017 NanoDefine is funded by the European Community's Seventh Framework Programme under Grant
Anna Katarzyna Undas (RIKILT)
NanoDefine is funded by the European Community's Seventh Framework Programme under Grant Agreement-604347
Wageningen
is your innovative partner for safe and authentic food. We are specialized in (forensic) measurements, perform top level research and by arrangement 24/7 available in case of emergencies
Expertise areas:
Wageningen
RIKILT coordinated EU-projects NanoLyse and NanoDefine and was a research partner in many more EU projects focusing on nanotechnology
Nanomaterial EU definition: “A natural, incidental or manufactured material containing particles, in an unbound state or as an aggregate or as an agglomerate and where, for 50 % or more of the particles in the number size distribution,
size range 1 nm - 100 nm.”
Validation based on:
5 days, n=3 (LOD,LOQ, n=5)
TiO2 in sunscreen Al2O3 in toothpaste Working range 20 – 500 nm 48 – 500 nm Repeatability (RSDr) [%] 2.4A, 8.0B, 19.9C 5.3A, 5.8B, 2.3C Intermediate precision (RSDRL) [%] 4.0A, 16.5B, 21.3C 15A, 24B, 29C LOD LODs 20 nm LODc 12 mg/kg prod. (10 peaks) LODs 48 nm LODc 61 mg/kg prod. (10 peaks) LOQ LOQs 22 nm LOQc 30 mg/kg prod. (30 peaks) LOQs 70 nm LOQc 180 mg/kg prod. (30 peaks) Measurement uncertainty [%] 5A, 25B, 33C 17A, 25B, 33C
A particle diameter, B particle number conc., C particle mass conc.
Product Median size [nm] a 154 b 126 c 143 d 140 e 123 f 110 g 143 h 106
This project has received funding from the European Union’s Seventh Programme for research, technological development and demonstration under grant agreement No 604347