Birck Nanotechnology Center BNC 105: Orientation & Welcome - - PowerPoint PPT Presentation

BNC 105: Orientation & Welcome

Birck Nanotechnology Center

Course Overview

• Introductions
• Facility Overview
• General Lab Safety
• BNC Specific policies
• Right-To-Know (RTK)

“New User” information

As a new user, you can use this link to find information for Birck.

http://www.nano.purdue.edu

Facility

• 21,296 square feet of laboratory

– Heavy Equipment Labs (MBE, CVD, Optics, High Accuracy) – Light General Labs (Biological, Chemical, Characterization) – 88 laboratory modules

• 25,252 square feet of cleanroom

– Semiconductor Fabrication Cleanroom – Pharmaceutical-Grade Cleanroom – ISO Class 3, 4, 5 (Class 1, 10, 100) – Bay-Chase Design

Scale of Things

10-2 m 10-3 m 10-4 m 10-5 m 10-6 m 10-7 m 10-8 m 10-9 m 10-10 m 1 cm 1 mm 100 µm 10 µm 1 µm 100 nm 10 nm 1 nm 0.1 nm

Natural World Manmade World

Modified from DOE file http://www.er.doe.gov/bes/scale_of_things.html

microscale nanoscale

I SO 14644-1 Class FED-STD- 209E Class 8 100,000 7 10,000 6 1,000 5 100 4 10 3 1

What is a Cleanroom?

0.5µm particles per meter cubed 0.5µ particles per foot cubed 3,520,000 100,000 352,000 10,000 35,200 1,000 3,520 100 352 10 35 1

• Administrative
• Faculty
• Laboratory and Cleanroom engineers

– Emergency response team

• Physical facilities
• Housekeeping
• Users (students, post docs, visiting scientists)
• Visitors

The Birck Team

Laboratory Orientation

Labs on the First Floor

Laboratory Orientation

Labs on the Second Floor

ID Card Coding Process

1. Complete safety training

• BNC 105 -- General Orientation
• BNC 150 -- Safety Fume Hood Training
• Special Hazard Training (only when needed)

2. Email from F.I.C. (Faculty in Charge) of lab to Mary Jo Totten (tottenm@purdue.edu) that you are authorized to enter lab and your card will be activated.

3. Make appointment with Mary Jo to meet in BRK 1220 for ID Card creation

Access to labs

ALL other training sessions are requested by contacting individual staff members.

New User Process Presentation

Cleanroom Processes

• All new processes will be reviewed by the

Birck engineering staff

• New users schedule time with the staff to

present and discuss their process prior to requesting training on new equipment

• Contact Kenny Schwartz,

kfschwar@purdue.edu, to schedule a meeting

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Birck Wiki – Wealth of Info

https://wiki.itap.purdue.edu/display/BNCWiki/BNCWiki+Home

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Birck iLabs

https://purdue.ilabsolutions.com/homepage

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iLabs – CHA Schedule Example

Our biggest concern is your safety!!! Evacuation Procedures:

• 1. When the alarm sounds leave the building immediately through the nearest exit.
• 2. Alert others to the emergency and ask if they will need help in evacuation.
• 3. Do not use elevators unless instructed to do so by emergency personnel.
• Proceed to the Southeast entrance of Burton Morgan Center
• If the Burton Morgan Center is closed (after-hours) then

proceed to the police station lobby.

Safety and Emergency Response Procedures

Laboratory Orientation

BNC Fire Alarm

• IMMEDIATELY evacuate the building using

the nearest exit

– Do not use the elevators – Ask others in your area if they need assistance

BNC Toxic Gas Alarm

• IMMEDIATELY evacuate the building
• Use the North, South, and East exits

– Do NOT exit by the gas rooms

• Do not use the elevators

1st Floor Evacuation Routes

2nd Floor Evacuation Routes

Evacuation Meeting Point

State Street Jischze Drive Birck Nanotechnology Center

Bindley Biosciences Center Burton Morgan Housing parking lot

Purdue Police Station

(use in the event Burton Morgan Is closed – after hours)

1 2

Tornado/Take Cover Alarm

• Move to a designated storm safe

area

• Stay away from windows
• Do not call 911 unless you

require emergency assistance

Laboratory Orientation

Safety and Emergency Response Procedures

Tornado Shelter Areas

Laboratory Spills All spills in the laboratory must be reported to a Laboratory Staff member immediately to remediate the spill as quickly as possible. This includes biological materials. Safety and Emergency Response Procedures

Laboratory Orientation

Bodily Fluid Spills Do not try to clean this up. Follow the Purdue University Blood-borne Pathogen procedures. Medical Emergency

• 1. Call 911 or use the Emergency Call Box to report the

incident.

• 2. Don’t move the victim unless safety dictates.

Safety and Emergency Response Procedures

Laboratory Orientation

Policies

• Building Emergency Plan can be found at:

– https://www.purdue.edu/discoverypark/birck/operations/safety.php and click on the Building Emergency Plan link under “Helpful Safety Links” at the bottom of the page.

• Lab access

– Training is required for escorted access to the labs. – Visitors are allowed

• Lab visitors must be accompanied at all times by a certified lab

user.

– Visitors may not handle Hazardous Materials or Equipment

All personnel entering the Birck Nanofabrication Laboratories are required to wear:

• Fully enclosed shoes
• Full leg covering – long pants & skirts
• Safety glasses (in labs marked as required)

– Personnel entering the Nanofabrication Laboratories must not wear contact lenses.

• Working with chemicals and in fume hoods require

additional PPE

Policies

• Pouring chemicals

– Splash proof goggles, face shield, chemical resistant apron and gloves

• Chemicals (fume hoods)

– There are two types of fume hoods, acid and solvent.

Policies

 NEVER PUT SOLVENTS DOWN DRAI NS

Policies

Electronic Ordering & Lab Supplies

 Ariba

– All chemical orders MUST have an up to date SDS attached to the order for approval by Steve Jurss (BNC Safety Officer) – All orders must be made using the University’s new electronic ordering system

 Lab Supplies delivered daily – give at least 24 hours

– Request supplies through Lorraine Fox foxl@purdue.edu – CR stocked in AM, Labs stocked in PM

Ordering Chemicals

• If you need to arrange training to place orders in

Ariba, please contact the BNC Business Office or Secretarial Staff. If there is enough interest in this training, they can arrange to have a class given on site.

• If you have questions in regard to the pre-

approved chemical list, please contact Stephen

• Jurss. If you have questions related to the
• rdering process, please contact the BNC

Business Office or Secretarial Staff.

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Gas Cylinders

• Gas cylinders must be changed by designated,

trained staff personnel.

• DO NOT attempt to change a gas cylinder.

– Contact staff before weekend run to verify gas level.

• NO hazardous process gas will be placed in a

laboratory

Laboratory Orientation

Gas and Chemical Delivery Procedures

Gloves are for your protection and the protection of the equipment or process

• Gloves may not be used to:

– Open doors – Answer Phones

Laboratory Orientation

Gloves

• Laser Laboratories

– The foremost concern is the danger to one’s eyes and exposed skin. The user must be trained and certified on working the laser and wear the appropriate eyewear protection. – Contact REM for laser safety training.

• Biology Laboratories

– For biological hazards, special training is necessary. – Contact REM for biological safety training.

• X-Ray sources

– Contact REM for X-ray safety training

Special Hazards

Policies

• No food or drinks in labs, galley or subfab.
• No Smoking anywhere in the building.
• PPE requirements are for all times

Citizenship Violations - Equipment

• The Birck disciplinary committee is comprised of two faculty

members, a staff scientist, a student representative, and the engineering manager. Policy and safety violations are first discussed between the engineering manager and the violator(s), after which the level of discipline is recommended to the committee, who determines the final disposition of the

• issue. The committee can decide penalties from restricted

access to suspension, depending on severity.

• All users are responsible for cleaning up after themselves and

for leaving their work areas ready for use by others.

• If any user is observed leaving a mess in a hood or near

equipment, or leaving an unattended tote not in its proper storage location, they will be subjected to mandatory participation in 4 hours of weekly staff support duties, or a

• ne-week suspension of all cleanroom privileges. This means

denied access to the cleanroom for one week.

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Citizenship Violations – Safety & Housekeeping

Questions?

Laboratory Orientation

RTK TRAINING

• The Purpose of this training is:

– Provide employees with knowledge to understand the

hazards of the chemicals they work with

– Provide a safer and healthier workplace for all employees – Ensure regulatory compliance with the State and Federal

Right-To-Know Law, 29 CFR 1910.1200

RTK TRAINING

• Who is covered under the RTK or Hazard

Communication Program (HCP or HazCom)

–

Support Service Employees:

• Physical Facilities
• Transportation
• Printing Services
• Airport Operations
• Intercollegiate Athletics
• Housing and Food Services
• Clerical

–

Academic Employees:

• Support Services (i.e... departmental shops)
• Laboratory with non-laboratory use of chemicals

–

An Employee is

• Anyone who receives a paycheck from

Purdue University

• Full-time, Part-time, Temporary, or

Student

RTK TRAINING

• To be informed about the known health

and physical hazards in your work area

• To be trained to use proper safety

techniques and hygiene practices

• To inform your DTI about accidents or

hazardous situations in your work area without fear of repercussions from your supervisor or the University

• To file a formal complaint with IOSHA

– Indiana Department of Labor Indiana

State Government Center South, Indianapolis, Indiana 46204-2287 317.232.2655

• To use the available information

and to stay informed about the hazards in your work area

• To use the safety techniques

and hygiene practices as a routine part of your daily activities

• To attend the training sessions

conducted by your DTI

Employee Rights Employee Responsibilities

RTK TRAINING

• OVERVIEW

– Hazardous Chemicals Used In

This Work Area:

• are listed on the chemical

inventory

• training may be done product by

product or by chemical class

– Chemical classes include but is

not limited to:

» acid » base » solvent

Job Specific Information

RTK TRAINING

• Chemical Hazards In This Work Area:

–

Solvents

• defatting of the skin
• eczema, severe dry and cracking skin
• examples: Actone, Methanol, Toluene, Dichlorobenzene

–

Acids, pH < 7

• burns and blisters the skin
• lung irritation if inhaled
• flush skin with tepid water for 15-20 minutes
• examples: Sulfuric, Nitric, Hydrochloric, Hydrofluoric, Acetic

–

Bases, pH > 7

• burns skin, damage area can penetrate to the bone if not neutralized
• eye damage
• seek medical attention
• examples: Sodium Hydroxide, Tetramethylammonium Hydroxide

–

Others

• Cryogens
• Pyrophorics
• Latex

RTK TRAINING

• Physical Hazards Of Products in the Work Area

– flammable – corrosive – reactive – explosive – cryogens

• Examples From This Work Area:

–

Acetone, Hydrogen, Silane

• Hydrofluoric Acid, Buffered Oxide Etch (BOE), Nitric, Sulfuric, Hydrochloric, etc acids
• Acetic acid

–

Liquid Nitrogen

–

Nitrogen gas

Second-Degree Burn From Liquid Nitrogen (LN2)

Severe Contact Allergic Dermatitis

RTK TRAINING

GHS – Global Harmonization System

• What an SDS contains:

– Product Name – Health Hazards – Flammability – Hazard Ratings – What to do in an emergency – What is the odor and appearance – Other information appropriate for the

work area

– Exposure control and PERSONAL

PROTECTIVE EQUIPMENT

Safety Data Sheet (SDS)

• Labels

–

Incoming containers must be labeled by manufacturer or distributor

• Required minimum information

–

Product name

–

Manufacturer/distributor

–

Address

–

Hazard information –

Labels must be intact and attached to the container

–

Prominently displayed on the container and at least written in English

–

Never remove or deface labels unless container is empty

–

Inspect containers on a regular basis to ensure labels are secure and still legible

• If label is partially coming off, reattach with adhesive or clear

packing tape

• If label is becoming illegible, use an approved University

secondary container label to re-label the container

–

If you transfer a chemical to a new container, it must labeled with:

Required minimum information

–Full Chemical name –Date –Your name

RTK TRAINING

GHS – Global Harmonization System

• NFPA Hazard Rating System

– diamond divided into 4 smaller

diamonds

• start at the left diamond move clockwise to

read the hazard information

• may or may not be color coded
• information will always be in the same location

–

health

–

fire

–

reactivity

–

special hazard

• numbers will be 0-4

–

0 = minimal hazard

–

4 = severe hazard

–

refer to pages 41-43 of the written compliance manual for complete definitions

• special hazard information includes oxidizer,

corrosive, acid, base, etc...

Labels, Continued

0-4 0-4 0-4

RTK TRAINING

GHS – Global Harmonization System

 Some old familiar labels

and numbering systems will become less used

 Some new classifications, new numbering

systems, and new “label elements” and labels will become what we teach and learn

 MSDSs will be called SDSs  Section 2 will provide

• Classifications
• Label elements

▪ Pictograms ▪ Signal word ▪ Precautionary statement ▪ Hazard statements Danger, or Warning, or no word

 Teaching and learning the meanings of the

GHS:

• Classifications
• Label elements

▪ Pictograms ▪ Signal word ▪ Precautionary statement ▪ Hazard statements P210: Keep away from heat/sparks/open flames/hot

• surfaces. - No smoking.

H225: Highly flammable liquid and vapor.

RTK TRAINING

• Control Methods

– ways to reduce exposure to chemical

products

• personal protective equipment

–

gloves

–

goggles

–

respirators

–

• ther
• engineering

–

local exhaust ventilation

–

remote handling of materials

• administrative

–

limit work time

–

rotate work groups

–

break areas separate from work areas

–

no smoking, eating, drinking, or applying cosmetics in work area

Effectiveness of PPE

RTK TRAINING

• LOCAL

– Involves one site in the body, usually the

point of contact

• Skin irritation or burns
• Eye irritation or burns
• Upper respiratory tract irritation
• SYSTEMIC

– Involves more than one part of the body,

not just the point of contact

• Central nervous system:

– headaches, dizziness, nausea, etc.

• Organ damage: liver, lungs, etc.
• Cancer

Star City 9-1 Window Cleaner

RTK TRAINING

• SUMMARY

– The written compliance manual, SDSs,

and chemical inventory are located at: Cleanroom entrance, Subfab, each lab galley.

– All containers must be labeled – Secondary labels available from DTI – The DTIs for your work area are: Steve,

Tim, Dave, Ron

– **Ask questions if you’re not sure**

Birck Orientation Training Successfully Completed