Welcome to Michigan Welcome to Michigan State University State - - PowerPoint PPT Presentation

welcome to michigan welcome to michigan state university
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Welcome to Michigan Welcome to Michigan State University State - - PowerPoint PPT Presentation

Welcome to Michigan Welcome to Michigan State University State University SEMED SEMED Scanning canning E Electron lectron S Microscope icroscope Ed Education ucation M Program Program Sponsored by the National Science Foundation


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SLIDE 1
  • SEMED

Welcome to Michigan Welcome to Michigan State University State University SEMED SEMED

S Scanning canning E Electron lectron M Microscope icroscope Ed Education ucation Program Program

Sponsored by the National Science Foundation (NSF)

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SLIDE 2
  • SEMED

Definition Definition

  • Motivational science program
  • Established in 1991 by Air Force

Research Laboratory (AFRL) Materials Directorate

  • Initiated at Alfred University in

2002

  • Local junior and senior high school

students and their teachers

  • Spend time learning about and

using latest technology in scanning electron microscopes (SEMs)

  • Started at Michigan State

University in 2002

Earwig Earwig SEM SEM SEMED Session SEMED Session Bumble Bee Bumble Bee Tongue Tongue

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SLIDE 3
  • SEMED
  • Demonstrate that science is fun
  • Show that scientists and

engineers are real people

  • Identify career opportunities in

science and engineering

  • Provide teachers with resources

in electron microscopy

  • Demonstrate how science is used

in a working environment

  • Establish a connection between

the classroom and the real world

Goals Goals

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SLIDE 4
  • SEMED
  • Rare opportunity for students

and teachers

  • Hands-on experience with the

latest high tech equipment

  • Fun and informative
  • Students meet and work with

scientists and engineers

  • Run by MSU volunteers
  • Conducted at the end of the

work day

Mosquito

Description Description

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SLIDE 5
  • SEMED
  • Informational meeting for

teachers at start of school year

  • Teachers meet the volunteers
  • Program organization discussed
  • Teachers sign up for sessions
  • Teachers taken through a typical

session

  • SEMED representative contacts

teacher several weeks prior to scheduled session to confirm

Ant Leg Ant Leg

Organization Organization

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SLIDE 6
  • SEMED
  • A Challenger Center survey revealed

teachers desired working with SEMs above any other scientific instrument

  • Challenger Center contacted the AFRL

Materials Directorate

  • Meetings were conducted and a formal

program was conceived and implemented

  • Students responded positively to hands-
  • n work only
  • Program was quickly adapted to fill

customer needs

Program History Program History

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SLIDE 7
  • SEMED
  • Twenty-two sessions per year
  • Expand number of schools

involved

  • Tech Trek - SEMED on wheels

Current and Future Status at AFRL Current and Future Status at AFRL

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SLIDE 8
  • SEMED
  • Teachers arrive with students and

are greeted by SEMED Volunteers

  • Volunteers introduce themselves

and talk briefly about what they do

  • Group is given a 20 minute talk on

what makes the microscopes work and what they are used for

Session Description Session Description

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SLIDE 9
  • SEMED
  • Group goes to lab

(4-6 students per SEM)

  • Volunteers explain how to operate

the microscopes

  • Volunteers stand back and let the

students drive

  • Typical session lasts about 1.5 hr
  • Students are encouraged to

explore

  • Specimens are provided

Session Description Session Description

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SLIDE 10
  • SEMED
  • Excites teachers, parents and

STUDENTS

  • Motivates students to consider

science as a career

  • Increases exposure of Michigan

State University to local region

  • Increases volunteerism

SEMED SEMED

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SLIDE 11
  • SEMED
  • 5-1000x
  • Two dimensional - limited

depth of focus

Mitochondria in Paramecium

Light Microscope Light Microscope

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SLIDE 12
  • SEMED
  • 10-75,000x
  • Surface textures

Mold spores on a leaf

Scanning Electron Microscope Scanning Electron Microscope (SEM) (SEM)

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SLIDE 13
  • SEMED

Leica 360 SEM Leica 360 SEM

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SLIDE 14
  • SEMED

Scanning Electron Microscope (SEM) Scanning Electron Microscope (SEM)

  • Phillips 515
  • Phillips 515

Phillips 515

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SLIDE 15
  • SEMED
  • Electron Backscatter Diffraction(EBSD)

Electron Backscatter Diffraction(EBSD)

  • Samples Polished thru 0.06µm finish; 20 minutes w/colloidal silica.
  • The 3 Sheet Orientations were investigated.
  • EBSD performed on a Phillips 515 SEM with LaB6 filament
  • 0.5µm step size; typical area mapped: 400µmx300µm.

L F F – Rolling Face CS – Cross Section L - Longitudinal CS Rolling Direction

Digiview Camera SEM Chamber

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SLIDE 16
  • SEMED

Electron Electron Electron Electron Orbit Orbit Nucleus Nucleus

Bohr’s Atom Bohr’s Atom

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SLIDE 17
  • SEMED

Electron Gun Electron Gun

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SLIDE 18
  • SEMED

Filament Cup Anode Electron Stream

Electron Gun or Filament Electron Gun or Filament

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SLIDE 19
  • SEMED

Electromagnetic Lenses Electromagnetic Lenses

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SLIDE 20
  • SEMED

Electromagnetic Electromagnetic Lenses Lenses

)

“Focus the stream into a beam”

Electromagnetic Lenses Electromagnetic Lenses

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SLIDE 21
  • SEMED

SEM SEM

Vacuum Chamber Electron Filament Anode Condenser Lens Scan Coils Secondary Electron Detector Specimen Scanning Beam

=

SEM Construction SEM Construction

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SLIDE 22
  • SEMED

Vacuum Tube Electron Filament Anode Condenser Lens Scan Coils Phosphor Scanning Beam

Television Television

Screen

SEM SEM

Vacuum Chamber Electron Filament Anode Condenser Lens Scan Coils Secondary Electron Detector Specimen Scanning Beam

Television vs. SEM Television vs. SEM

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SLIDE 23
  • SEMED

Secondary Electron Primary Electron Primary Electron

Secondary Electrons Secondary Electrons

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SLIDE 24
  • SEMED

Primary Electrons Secondary Electron Detector Secondary Electron Escapes to detector Secondary Electron loses energy and is reabsorbed Sample Surface

Secondary Electron Detection Secondary Electron Detection

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SLIDE 25
  • SEMED

Secondary Electron Detector Image Secondary Electron Detector Image

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SLIDE 26
  • SEMED

Backscattered Electrons, are Electrons from the incoming beam which have been Elastically Scattered back out of the sample. The number of backscattered Electrons generated increases with the Atomic Number of the specimen.

Backscattered Electron Detection Backscattered Electron Detection

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SLIDE 27
  • SEMED

Example of a Secondary Electron Image and a Backscattered Electron image. The image is from the glaze body interface of a coffee cup Notice that the glaze is much brighter in BSE and that there are crystals in the glaze which are seen in the BSE image and not in the SE image. Another thing to observe is the particle of dust ( very low atomic number ) seen in the SE image is not seen in the BSE image. Also, you can see bright rims around the pores in the SE image which are not present in the BSE image

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SLIDE 28
  • SEMED

Characteristic X-Ray

Characteristic X Characteristic X-

  • Ray

Ray

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SLIDE 29
  • SEMED

X X-

  • ray Production Diagram

ray Production Diagram

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SLIDE 30
  • SEMED

Top six pictures show earwig parasites Bottom two pictures are of a sand dollar

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  • SEMED
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SLIDE 32
  • SEMED
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SLIDE 33
  • SEMED
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SLIDE 34
  • SEMED
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SLIDE 35
  • SEMED
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SLIDE 36
  • SEMED