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The Search for Improved Wavelength Shifting Plate Performance - - PowerPoint PPT Presentation

The Search for Improved Wavelength Shifting Plate Performance Stuart Mufson, Brice Adams, Brian Baugh DUNE Photon Detector Workshop May 17, 2016 Motivation: The properties of the photon detectors are separable and can be studied/optimized


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SLIDE 1

The Search for Improved Wavelength Shifting Plate Performance

Stuart Mufson, Brice Adams, Brian Baugh DUNE Photon Detector Workshop May 17, 2016

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SLIDE 2

Motivation: The properties of the photon detectors are separable and can be studied/optimized independently. These PD properties include –

  • 1. attenuation length
  • a. Eljen light guides are a commercial product

with uniformly excellent attenuation length (> 2m)

  • b. issue resolved for IU technology
  • 2. brightness
  • a. relative brightness
  • optimization of wavelength shifting plates
  • b. absolute brightness/efficiency
  • 3. SiPM aging
  • a. reasonable performance in IU tests
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SLIDE 3

Testing Plan:

  • 1. Establish technology performance @ 128 nm in

VUV monochromator

  • (relatively) rapid method for testing/comparing

many technologies

  • 2. Show that technology performance in VUV monochromator

correlates with performance in liquid argon without Eljen light guide

  • setup in local dewar at IU: α source/plate technology/SiPM
  • 3. Test performance with Eljen light guides to demonstrate

PD system performance in local dewar

  • if feasible, test at Fermilab in TallBo/Blanche under

under controlled conditions

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SLIDE 4

Search Matrix

* TallBo plates IU solution: TPB, DCM MIT: TPB, toluene, acrylic, alcohol

°

substrate method of application wavelength shifting solution 1side/2side acrylic 1/16" spray/bake IU 1 side polycarbonate 1mm paint MIT polycarbonate 0.004" dip coated heat shrink (Walmart) spray heat shrink 0.001" HVLP vinyl sheet by hand vinyl 1/16" mylar 0.004" saran wrap fused silica crystal quartz

* * * *

°

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SLIDE 5

VUV Monochromator Measurements

  • McPherson model 234 VUV Monochromator with H2 lamp
  • Vacuum connection to a turbo pump, pumped down

to purge N2, O2, H2O

  • Backfilled with pure gaseous argon (slightly overpressured)
  • Calibrate H2 lamp with NIST calibrated photodiode

VUV light

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SLIDE 6

Issues:

  • MgF2 window becomes less transparent with exposure to

128 nm light

  • characterize technology performance with metric:

( waveshifted optical light as measured by SiPM)/ (128 nm light as measured by NIST photodiode)

0.0E+00 5.0E-10 1.0E-09 1.5E-09 2.0E-09 2.5E-09 3.0E-09 3.5E-09 4.0E-09 3/11/16 3/21/16 3/31/16 4/10/16 4/20/16 4/30/16 5/10/16 5/20/16

VUV (current - dark current) [A]

VUV current measured by NIST photodiode vs date: cleaned 3/21; 4/1; 4/14; 5/3

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SLIDE 7

y = 65950x-0.438

0.E+00 1.E+04 2.E+04 3.E+04 4.E+04 5.E+04 6.E+04 7.E+04 5 10 15 20 25 30 35 40 45 50

y = 0.0001x + 1.0089

0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 5 10 15 20 25 30 35 40 45 50

Issues:

  • Monitor systematics by continuously measuring a standard

wavelength shifting plate: sprayed/baked acrylic plate, similar to TallBo #5 plate

  • radiation damage to standard, when corrected, shows stable

system performance (SiPM current – dark current)/ ( VUV current – dark current) corrected for radiation damage

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SLIDE 8

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 1 6 11 16 21 26 31 36 41 46 51 56 62 67 72 77 82 87 92 97 102

SiPM current/VUV current measurement

SiPM current/VUV current

Summary of all technologies tested:

  • measurement standard red
  • TallBo #5 waveshifting plates (Denver’s talk) blue
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SLIDE 9

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 1 6 11 16 21 26 31 36 41 46 51 56 62 67 72 77 82 87 92 97 102

SiPM current/VUV current measurement

SiPM current/VUV current

SiPM current/VUV current

Entries 104 Mean 1.559 RMS 1.526

1 2 3 4 5 6 7 8 10 20 30 40 50

SiPM current/VUV current

Entries 104 Mean 1.559 RMS 1.526 SiPM current/VUV current for all technologies tested

Summary of all technologies tested:

  • measurement standard red
  • TallBo #5 waveshifting plates (Denver’s talk) blue
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SLIDE 10

0.00 1.00 2.00 3.00 4.00 5.00 6.00 1 3 5 7 9 11

SiPM current/VUV current

1/16" acrylic, sprayed & baked TallBo plates solid

SiPM current/VUV current

Entries 104 Mean 1.559 RMS 1.526

1 2 3 4 5 6 7 8 10 20 30 40 50

SiPM current/VUV current

Entries 104 Mean 1.559 RMS 1.526 SiPM current/VUV current for all technologies tested

Sprayed/Baked technology used in TallBo #5:

  • sprayed with computer controlled spray apparatus,

baked at 80 C

  • good performance with room for improvement over

TallBo performance

  • VUV enables QC to select best performance
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SLIDE 11

0.0 1.0 2.0 3.0 4.0 5.0 6.0 1 3 5 7 9 11

SiPM current/VUV current

Heatshrink (Walmart), dipped, brushed, sprayed

SiPM current/VUV current

Entries 104 Mean 1.559 RMS 1.526

1 2 3 4 5 6 7 8 10 20 30 40 50

SiPM current/VUV current

Entries 104 Mean 1.559 RMS 1.526 SiPM current/VUV current for all technologies tested

Heat shrink material (Walmart) shows best consistent performance

  • currently being tested at MTS for contamination issues
  • has only been fixed to small samples of Eljen light guides
  • promising but obviously needs some work
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SLIDE 12

3 SensL SiPMs Am241 5.5 MeV α LAr dewar wavelength shifting plate

  • 2. Show that technology performance in VUV monochromator

correlates with performance in liquid argon without Eljen light guide

  • setup in local dewar at IU: α source/plate technology/SiPM

1000 2000 3000 4000 5000 6000 7000 8000 9000 1 2 3

ADC counts SiPM position

Comparison of Wavelength Shifting Plates in LAR

TallBo plate heat shrink

performance in LAr correlates with performance in VUV

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SLIDE 13
  • 3. Test performance with Eljen light guides to demonstrate

PD system performance in local dewar

  • preliminary studies encouraging, more work needed

second α source added 3 SensL SiPMs

3-day turnaround

  • 1. light guides loaded

into frame

  • 2. dewar pumped down
  • vernight; backfilled

with gaseous Ar

  • 3. LAr fill and

measurements

  • 4. warm up
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SLIDE 14

Eljen Light Guide/Wavelength Shifting Plate QC Plans Eljen light guides:

  • commercial product, if made correctly, will work
  • attenuation length measured > 2m multiple times at room

temperature and in LAr

  • test in dark box at room temperature
  • demonstrate correlation between dark box and LAr

Wavelength shifting plates:

  • demonstrated that VUV monchromator wavelength performance

at room temperature correlates with performance in LAr

  • current work at IU concerns uniformity over 3 3/8” x 12”

wavelength shifting plates as a function of technology

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SLIDE 15

Conclusions

  • demonstrated that technology performance @ 128 nm can

be studied in VUV monochromator

  • performance in VUV correlates with performance in LAr
  • two technologies have been identified as improving the

performance as see in TallBo #5

  • preliminary studies are encouraging that wavelength shifting

plates work efficiently with Eljen light guides

  • QC plans are being developed for both wavelength shifting

plates and Eljen light guides