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Testing for Rotational Moulding (RM) and Service Capabilities of BITS BITS Pilani Dr. Sachin Waigaonkar K K Birla Goa Campus Outline About BITS Pilani Different Quality Tests in Rotational Moulding Service Capabilities for


  1. Testing for Rotational Moulding (RM) and Service Capabilities of BITS BITS Pilani Dr. Sachin Waigaonkar K K Birla Goa Campus

  2. Outline • About BITS Pilani • Different Quality Tests in Rotational Moulding • Service Capabilities for Rotational Moulding Industry. • Conclusions BITS Pilani, K K Birla Goa Campus

  3. BITS Pilani-Four Accredited Campuses Dubai Campus (2000) Pilani Campus (1964) Goa Campus(2004) Hyderabad Campus(2008) BITS Pilani, K K Birla Goa Campus

  4. University – Industry Linkage Practice School Programmes Committed to University – Industry Collaboration Since its inception (1964) Practice in Theory learnt Industry in classroom As on today, Collaboration with 300+ industries BITS Pilani, K K Birla Goa Campus

  5. University – Industry Linkage Work-Integrated Learning and Collaborative Programmes [20,000 students on roll | 30,000 students graduated] 33 Organizations | 24 Degree Programmes BITS Pilani, K K Birla Goa Campus

  6. T esting in Rotational Moulding • Testing of Raw Materials:  Testing of Pellets and  Testing of Powder • Testing of Product.( Fit, Form and Function) • Long Term Testing of RM Products. • Advanced Tests for Material Development BITS Pilani, K K Birla Goa Campus

  7. T esting of Raw Material (Pellets): • Density • Melt Flow Index (MFI) • Shape, Size Colour of Pellets • Tensile Strength / Modulus • Flexural Modulus • Heat Distortion Temperature (HDT) • Environmental Stress Cracking Resistance (ESCR) BITS Pilani, K K Birla Goa Campus

  8. Powder Characterization • Dry Flow Test • Bulk Density Test • Sieve Analysis - Particle Size Distribution • Microscopic View for Characterization of Powder. BITS Pilani, K K Birla Goa Campus

  9. T esting of form features of the product: • Dimensions of Product • Profile • Angularity • Depth • Wall Thickness Distribution • Shrinkage and Warpage BITS Pilani, K K Birla Goa Campus

  10. Mechanical Properties of the product: • Density of part • Tensile Strength and Modulus • Flexural Strength and Modulus • Low Temperature Impact Strength • HDT • ESCR • Gel Cure Test (XLPE), etc. BITS Pilani, K K Birla Goa Campus

  11. Long T erm and Advanced T esting • Colour Testing in Light booth • Weatherability using Xenon Arc Lamp • Differential Scanning Calorimetry (DSC) • Dynamic Mechanical Testing Creep Testing using DMA • Thermal Gravimetric Analysis (TGA) • Scanning Electron Microscopy (SEM) • Compounding Studies using Torque Rheometer. • Rheological Studies using Parallel Plate rheometry A few important tests are discussed here BITS Pilani, K K Birla Goa Campus

  12. Density • The specific gravity or density is a property measured to:  Identify a material,  Follow physical changes in a sample,  Indicate degree of uniformity among different sampling units or specimens.  To calculate strength-weight and cost-weight ratios. BITS Pilani, K K Birla Goa Campus

  13. Effect of Density on Different Properties # • Tensile Strength • HDT • Stiffness • Shrinkage • Hardness • Barrier Properties Property • Chemical Resistance • Impact Strength • ESCR • Optical Properties • Ductility Density #: Ref: R.J. Crawford, Rotational Moulding, Rapra Review Report, 71 BITS Pilani, K K Birla Goa Campus

  14. Testing of Density • Ref: ASTM D-792 or ISO 1183 method D. BITS Pilani, K K Birla Goa Campus

  15. T esting of Powder: Dry Flow and Bulk Density Ref: Association of Rotational Molders, Test Method for Flowability and Apparent Density of Polyethylene Powders, Version 2.1 – November 2011, pp-2-8, ASTM 1895-69 with conditions redefined for use in rotational moulding BITS Pilani, K K Birla Goa Campus

  16. Melt Flow Index (MFI) Dynisco MFI in Our Lab Schematic Ref: ASTM D -1238 BITS Pilani, K K Birla Goa Campus

  17. Effect of MFI on Different Properties # • Flow Properties e.g. Viscosity Property • Impact Strength • Tensile Strength • ESCR • Weatheribility • Chemical Resistance • Ductility MFI #: Ref: R.J. Crawford, Rotational Moulding, Rapra Review Report, 71 BITS Pilani, K K Birla Goa Campus

  18. ESCR Ref: ASTM D-1693 BITS Pilani, K K Birla Goa Campus

  19. T esting of T ensile Properties UTM in Lab (Load Cell 0-10 KN) Typical Stress-Strain Plot Ref : ASTM D 638 BITS Pilani, K K Birla Goa Campus

  20. T esting of Flexural Properties Schematic of Flexural Testing Lab Testing Set Up Ref : ASTM D 790 BITS Pilani, K K Birla Goa Campus

  21. Typical Flexural Curves Ref : ASTM D 790 BITS Pilani, K K Birla Goa Campus

  22. Schematic of Low T emp. Impact T est Ref: ARM Low Temperature Impact Test BITS Pilani, K K Birla Goa Campus

  23. HDT : Schematic and Set Up Schematic of Flexural Testing Lab Set Up for HDT Ref: ASTM D 648 BITS Pilani, K K Birla Goa Campus

  24. Geometry and Form T esting: Coordinate Measuring Machine (CMM) Testing of product for Dimensions, Profile, Depth, Angularity, etc. BITS Pilani, K K Birla Goa Campus

  25. Other Facilities at BITS GOA ( will be replaced with Photos) • Dynamic Mechanical Analyzer (DMA): TA Instruments USA • Differential Scanning Calorimetry (DSC). • Thermo gravimetric Analysis (TGA) • Scanning Electron Microscope • Templogger • Injection Moulding Machine: Ferromatic Millerkon -50 T • Compression Moulding Press-32 T • 3-D printer for Rapid Prototyping: Make Stratasys • ROTOSIM. • Pro-E, ANSYS and other CAE tools. BITS Pilani, K K Birla Goa Campus

  26. Conclusion: Our Service Capabilities Test Standard Density ASTM D 1505/D-4883/D-792 or ISO 1183 method D. Dry Flow and Bulk Density ASTM 1895-69 with conditions redefined for use in rotational moulding MFI ASTM D -1238 ESCR ASTM D-1693 Tensile Strength and Modulus ASTM D 638 Type I to IV Flexural Strength and Modulus ASTM D 790 Low Temperature Dart Impact ARM International HDT ASTM D 648 BITS Pilani, K K Birla Goa Campus

  27. Thanks “ The best Research will give the best Teaching and the best Teaching will give the best Research” Dr. APJ Abdul Kalam. BITS Pilani, K K Birla Goa Campus

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