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PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 - PDF document

PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 Courtney Phillips Wednesday, March 14, 2012 For more information, contact courtney.phillips@perkinelmer.com 1 PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14,


  1. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 Courtney Phillips Wednesday, March 14, 2012 For more information, contact courtney.phillips@perkinelmer.com 1

  2. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 ������������ ��������� ������� Federal ��������� FDCA Food, Drugs & Cosmetics �������������� Federal Act Insecticide, ���������� FIFRA Fungicide & Rodenticide ���������� Act For more information, contact courtney.phillips@perkinelmer.com 2

  3. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 For more information, contact courtney.phillips@perkinelmer.com 3

  4. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 For more information, contact courtney.phillips@perkinelmer.com 4

  5. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 SPE ����������� Quechers Dilution Automated variants ���������� Liquid Chromatography* ��������� MS/MS High Resolution Mass Analyzer SPE ����������� Quechers Solid Phase Extraction Separates analytes of interest Dilution from a complex matrix Phases similar to LC columns Automated variants Requires vacuum manifold ~ 5 – 10 min/sample ���������� Liquid Chromatography* ��������� MS/MS High Resolution Mass Analyzer For more information, contact courtney.phillips@perkinelmer.com 5

  6. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 SPE ����������� Quechers Dilution Quick, Easy, Cheap, Effective, Rugged & Safe Developed specifically for Automated variants pesticides analysis in foods Created as an alternative to the Luke method Requires centrifuge ~ 5 – 10 min/sample ���������� Liquid Chromatography* ��������� MS/MS High Resolution Mass Analyzer SPE ����������� Quechers Dilution Automated variants ���������� Liquid Chromatography* Considerations for Liquid Chromatography Mass analyzers require lower flow rates UHPLCs have the ability to run at these flow rates ��������� MS/MS However, traditional UHPLC columns may not be ideal – Consider Superficially Porous Particle (SPP) columns High Resolution Mass Analyzer For more information, contact courtney.phillips@perkinelmer.com 6

  7. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 SPE ����������� Quechers Dilution Automated variants Triple Quadruple Instrument ���������� Liquid Chromatography* ��������� MS/MS High Resolution Mass Analyzer SPE ����������� Quechers Dilution Automated variants Time of Flight (TOF) Instrument ���������� Liquid Chromatography* ��������� MS/MS High Resolution Mass Analyzer For more information, contact courtney.phillips@perkinelmer.com 7

  8. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 LC-TOF Pesticides by LC-TOF Prometryne/dichloran Diazinon Acetamiprid Malathion/metalochlor Mevinphos isomers Mevinphos Oxamyl Dimethoate Acephate Spinosad A Methomyl Anilazine For more information, contact courtney.phillips@perkinelmer.com 8

  9. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 Pesticides by LC-TOF Pesticides by LC-TOF ������������������������������������������������ For more information, contact courtney.phillips@perkinelmer.com 9

  10. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 Spiked Pesticides in Celery Extraction by Quechers RP-LC Pos ion mode Dual probe ESI- TOF with lock mass calibration Carbendazim in Orange Juice RP-HPLC Brownlee C18 SPP 10cm m/z 100-400 Dual ESI Source with Lock Mass Gradient from 30% � � 100% MeOH � � 1.5 spectra/sec Drying Gas Flow 12 L/min Ambient temp, 0.3mL/min Flow Drying Gas Temp 350 o C Capillary exit voltage = 90 V For more information, contact courtney.phillips@perkinelmer.com 10

  11. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 Carbendazim in Orange Juice RP-HPLC Brownlee C18 SPP 10cm m/z 100-400 Dual ESI Source with Lock Mass Gradient from 30% � � � � 100% MeOH 1.5 spectra/sec Drying Gas Flow 12 L/min Ambient temp, 0.3mL/min Flow Drying Gas Temp 350 o C Capillary exit voltage = 90 V Carbendazim in Orange Juice RP-HPLC Brownlee C18 SPP 10cm m/z 100-400 Dual ESI Source with Lock Mass Gradient from 30% � � � 100% MeOH � 1.5 spectra/sec Drying Gas Flow 12 L/min Ambient temp, 0.3mL/min Flow Drying Gas Temp 350 o C Capillary exit voltage = 90 V For more information, contact courtney.phillips@perkinelmer.com 11

  12. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 Carbendazim in Orange Juice All data, all the time… For more information, contact courtney.phillips@perkinelmer.com 12

  13. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 All data, all the time… All data, all the time… For more information, contact courtney.phillips@perkinelmer.com 13

  14. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 LC-TOF ��������� �!�!"# For more information, contact courtney.phillips@perkinelmer.com 14

  15. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 For more information, contact courtney.phillips@perkinelmer.com 15

  16. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 For more information, contact courtney.phillips@perkinelmer.com 16

  17. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 For more information, contact courtney.phillips@perkinelmer.com 17

  18. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 For more information, contact courtney.phillips@perkinelmer.com 18

  19. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 ����$�������%&������&'��������(��)��*�"�����+&���� ������������������� ����'�������������� , �������-������.� �����������&'�� For more information, contact courtney.phillips@perkinelmer.com 19

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  22. PerkinElmer talks at spring TCJJP Meeting Wednesday, Mar. 14, 2012 /&�������6 For more information, contact courtney.phillips@perkinelmer.com 22

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