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FYS5310/FYS9320 Electron Microscopy, Electron Diffraction and - - PowerPoint PPT Presentation
FYS5310/FYS9320 Electron Microscopy, Electron Diffraction and - - PowerPoint PPT Presentation
FYS5310/FYS9320 Electron Microscopy, Electron Diffraction and Spectroscopy II Spring 2018 Electron Microscopy, Electron Diffraction and Spectroscopy II Fultz & Howe. Transmission Electron Microscopy and Diffractometry of Materials. 4
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Electron Microscopy, Electron Diffraction and Spectroscopy II
- Fultz & Howe. Transmission Electron Microscopy and Diffractometry of
- Materials. 4th ed. Springer, 2013. [F&H]
– In particular chapters 4, 5, 12
- Williams & Carter. Transmission Electron Microscopy. 2nd ed. Springer,
- 2009. [W&C]
– In particular parts 3 & 4
- Various articles and papers (mandatory for PhD students)
- Handouts and lectures
- Ray Egerton. Electron Energy-Loss Spectroscopy in the Electron Microscope
- Pennycook & Nellist. Scanning Transmission Electron Microscopy: Imaging and
- Analysis. [P&N]
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Preliminary teaching schedule
Lectures: 2-4 hours per week Exercises and lab: 0-4 hours per week (on average 4 hours teaching per week)
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Preliminary teaching schedule
- Lectures on Thursdays 12:15-14:00
- Exercises and lab on Wednesdays 12:15-
16:00 (not every Wednesday)
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FYS5310 teaching schedule
Preliminary schedule only! You should keep the class-times on Wednesdays and Thursdays open unless notified by email (or in this schedule) that there is no class References to the textbook to Fultz & Howe unless stated otherwise.
Date Time Lecture/lab Topic Chapters Homework
Thursday 18.01.2017 12:15-14:00 Lecture Introduction to the course Wednesday 24.01.2018 12:15-16:00 Lab/Colloquium No class Thursday 25.01.2018 12:15-14:00 Lecture Derviation of the structure factor and the atomic form factor (01) 4.1, 4.3, 6.1 Wednesday 31.01.2018 12:15-16:00 Lab/Colloquium Going though exercise set 1 Exercise set 1 (handout) Thursday 01.02.2018 12:15-14:00 Lecture No class Wednesday 07.02.2018 12:15-16:00 Lab/Colloquium Going though exercise set 2 Excercise set 2 (handout) Thursday 08.02.2018 12:15-14:00 Lecture Uses of EELS and EELS instrumentation (02) 5.1, 5.2; W&C 37 Wednesday 14.02.2018 12:15-16:00 Lab/Colloquium Going though exercise set 3 Exercise set 3 (handout) Thursday 15.02.2018 12:15-14:00 Lecture Inelastic form factors (03) 5.4.1-5.4.3 + primer
- n Dirac notation
Wednesday 21.02.2018 12:15-16:00 Lab/Colloquium No class Thursday 22.02.2018 12:15-14:00 Lecture Inelastic form factors, scattering cross sections, dipole selection rules (04) 5.4.4-5.4.7, W&C 39, plus Brehm and Mullin on parity and dipole selectrion rules Wednesday 28.02.2018 12:15-16:00 Lab/Colloquium Thursday 01.03.2018 12:15-14:00 Lecture
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Interface termination in ZnO/Cu2O
1 n m
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- Parallell beam electron diffraction
- Convergent beam electron diffraction
- Brightfield and darkfield imaging
- High resolution imaging
- Brightfield scanning transmission electron microscopy
- Darkfield scanning transmission electron microscopy
- X-ray microanalysis composition analysis
- X-ray microanalysis elemental mapping
- Electron holography and phase reconstruction
- Electron energy loss spectroscopy
- Electron energy loss spectroscopic imaging and
mapping
- ++
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Electron beam – sample interaction
W&C
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Scattering with energy transfer
F&H
' k k E E
Inelastic scattering:
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Scattering without energy transfer
F&H
' k k E E
k0 k’ Dk
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Diffraction
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Bragg’s law
- Is this a good model?
– It’s simple – It «works»
- But does it capture the physics of what is