Improved process performance of flat dies by a much wider die gap - - PowerPoint PPT Presentation

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Improved process performance of flat dies by a much wider die gap - - PowerPoint PPT Presentation

Improved process performance of flat dies by a much wider die gap operation window and a new surface finish of the die body Otto Plassmann Session 4.2 paper 7697 Part 1 Improved die gap operating window Paper 4.2 Otto Plassmann 2 In the


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Improved process performance of flat dies by a much wider die gap

  • peration window and a new surface

finish of the die body

Otto Plassmann Session 4.2 paper 7697

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Paper 4.2 Otto Plassmann 2

Part 1 Improved die gap operating window

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In the extrusion coating technology the flat dies are always the handover tool of the melt from the extruder to the substrate, but in a well distributed way. So it is just normal that there are different solutions of these flat dies around the world. All dies have an opening slot, the die gap over the operating width, even if the internal design is totally different.

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So this paper will not discuss the various types

  • f flat dies and the length of the die land,

the last flow channel just before the exit.

  • T-slot
  • fish-tail
  • coat-hanger
  • dual slot
  • multiple manifold single slot
  • T-slot internal deckling
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The die gaps, we found in the market, were in a range from 0,3 up to 1,4 mm. The draw down ratio was for a certain period discussed everywhere. A lot of recommendations for different polymers were given.

Draw Down Ratio = Die gap in µm Coating thickness in µm

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Here some examples of draw down ratios, as we found more than 2 different philosophies.

Draw Down Ratio = Die gap in µm Coating thickness in µm 1000 1000 700 700 400 400 die gap in µm 100 10 100 10 100 10 coating thickness in µm 10 100 7 70 4 40 draw down ratio

It was common understanding to have a low draw down ratio, to allow a good die control and good coating profile in cross direction!! but …….

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But different types of polymers have a different behavior, which leads to a different die swell.

Draw down in theory Draw down in reality Here we have more draw down stress for the polymer melt thickness at the start of the draw down

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So the draw down ratio theory was in competition with the die swell, which is not so easy to measure or visualize. To ask for are a die gap recommendation was nearly impossible, as there were a lot of different opinions. By experience on our laboratory line, a die gap

  • f 1 to 1,2 mm gave good results and good

coating weight profiles for LDPE!

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T.C. T.C.

Die bolt Die bolt Adjustment Adjustment differential differential screw screw Distance holder Distance holder Flexible die lip Flexible die lip

Conventional automatic die

The die bolts realize an operating window for the die gap

  • f +- 0,2 mm around the mechanical fixed basic gap.
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By experience on our laboratory line a die gap

  • f 1 to 1,2 mm gave good results and

coating weight profiles for LDPE, but not for all other polymers! So we had very often to adjust the basic die gap, to a smaller value, to be able to run other polymers. This basic adjustment was very time consuming and is only acceptable for a laboratory coating line.

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Based on this experience there was the idea to enlarge the movement window for the die gap in an easy and convenient way. The die bolt movement capacity could not be enlarged, as this would mean a lower resolution for the final cross direction thickness control. So the distance holder was developed further to a second heating bolt, the so called Spacer, with the movement from the temperature related enlargement of the steel as well.

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T.C. T.C.

Automatic die with a fast die gap base adjustment

Temperature Temperature controlled controlled spacer spacer The spacers realize an operating window for the basic gap

  • f +- 0,2 mm around the mechanical fixed base position.
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Enlarged die gap operating window for the die gap

By setting the temperature of the spacers, we could achieve different basic die gaps.

Die gap 0,7 mm at medium spacer temperature Die gap 0,9 mm at high spacer temperature Die gap 0,5mm at low spacer temperature

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Total operating window of spacer and die bolt

Die gap at various spacer and die bolt temperatures in mm die bolt temperature Spacer- temperature low medium high high 0,3 0,5 0,7 medium 0,5 0,7 0,9 low 0,7 0,9 1,1

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How to find the best die gap The speed how fast and stable a good cross profile can be reached is a very good indicator to identify the best operating window. In addition to this, we have installed a pressure sensor at the die inlet channel. A too high internal melt pressure indicates a high die swell, which can lead to an uneven cross profile.

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Part 2 The new surface finish

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In the extrusion coating history the materials

  • f the flat-dies have gone through a long evolution.

Beside the base material of the die also the surface finish technology made its own evolution. And there is still another step of evolution to be mentioned here, which goes in hand with the improved performance of the enlarged die operating window technology, described in the few slides before.

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Here some well known surfaces

  • standard steel barefoot
  • stainless steel barefoot
  • stainless steel chromium plated
  • steel chromium plated
  • steel nickel plated
  • ….

The demand profiles and/or the applications were extremely different.

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Some requested properties

  • protection against corrosion
  • low or no tendency for deposits
  • easy flow of the polymer inside the die
  • good purging behaviour
  • low tendency for die lines
  • hard and robust surface, not to be

damaged during mechanical cleaning

  • ….
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Another property, which is tricky to measure Is the friction between melt and surface. Some people report about flow problems

  • r even a rough shark skin of the product.

This is the well known problem of melt fracture. Also the micro cracks of the chromium surface are made responsible for some purging or flow problems, as there are always some polymer deposits sitting in the micro cracks.

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The solution When we got our new die, now more than 1 year ago, we took the chance to get the new surface. This surface reduced dramatically or eliminated nearly all known problems reported before. It is a kind of chromium nitride plasma coating, which delivers this performance.

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The rainbow effect from the surface of this die lip indicates that it is something magic!

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Summary 1/2

  • With the adjustable basic die gap

via the spacer temperature different polymers can be coated in good quality without mechanical adjustments on the die

  • With monitoring and influencing the

melt pressure in the die, we have identified a new tool to improve the quality and processability

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Summary 2/2

  • The behavior of the melt pressure in the die

will be topic of another study

  • The new die surface supports a smoother

production and less deposits, die lines and cleaning problems

  • The new die generation allows a better

cleaning, due to the larger „cleaning gap“

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If you don‘t believe, come and see.

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Special Acknowledgment

  • Chris Barton

ER WE PA Davis Standard Germany

chris.barton@davis-standard.de

  • Uwe Fidersek

ER WE PA Davis Standard Germany

uwe.fidersek@david-standard.de

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Thank you for your Attention! Sorry for so much text and not enough pictures.

Otto Plassmann INEOS Polyolefins