DMRQA DMRQA DMRQA DMRQA
Presented by the Presented by the
Arizona Department of Health Services Arizona Department of Health Services
2010 2010
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DMRQA DMRQA DMRQA DMRQA Presented by the Presented by the - - PowerPoint PPT Presentation
DMRQA DMRQA DMRQA DMRQA Presented by the Presented by the Arizona Department of Health Services Arizona Department of Health Services 2010 2010 1 What is it? What is it? What is it? What is it? DMRQA DMRQA - - Discharge
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Annual program required under the National
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This is done through a proficiency evaluation
The study is not performed using routine
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All major permittees must participate in the
Selected minor permittees are required to
All major and minor permittees must
4 Participation differs for major and minors
2010 letters should have arrived late March or
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DMR-QA Letter Cover
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Letters mailed March and received
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Proficiency studies accepted opening Jan 1
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Results to Coordinator by Aug 20
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Unacceptable results corrective action report
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Immediately mail or email verification of letter receipt
Immediately mail or email verification of letter receipt to state coordinator to state coordinator
There is a date in the EPA letter for responses to be received p but even if received after the date, please respond but even if received after the date, please respond – there is there is no penalty in responding late for receipt of the letter no penalty in responding late for receipt of the letter
I f ti h t t id i il il i EPA I f ti h t t id i il il i EPA
Information on what to provide in mail or email in EPA
Information on what to provide in mail or email in EPA letter letter
Permit number and contact information
Corrections should be included if necessary
Corrections should be included, if necessary
Ensure the contact information for your facility is
Ensure the contact information for your facility is current on a routine basis current on a routine basis
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current on a routine basis current on a routine basis
Contact your state coordinator or ADEQ
All NPDES (AZPDES) permit holders are
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Send an email to the state coordinator
Send an email to the state coordinator
List facility permit number
List reason requesting exception List reason requesting exception List reason requesting exception
Contact information
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Compare what type of testing/analyte is
Chemistry/Microbiology/Analyte y gy y y gy y
WET Organisms/Test Conditions/End Points
Determine which ones were reported or will
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Chemistry/Microbiology Analyte Checklist DMR-QA Study 30
Each year the checklist may be y y slightly different as additional analytes are added. 13 13
Determine which compliance analytes you perform in
Determine which compliance analytes you perform in-
house and which are contracted
If your permit does not list an analyte that appears on the If your permit does not list an analyte that appears on the If your permit does not list an analyte that appears on the checklist, then you do not need to perform a proficiency for checklist, then you do not need to perform a proficiency for that analyte that analyte
Differences in Major and Minors
Differences in Major and Minors
Each facility that has what are called “15 minute” analytes that are tested for must follow the in house steps that are tested for must follow the in house steps p
Major permit holders must also contact contract laboratories
Minors permit holders only need to be concerned with “15 minute” minute”
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Ammonia, pH, turbidity, low
Ammonia, pH, turbidity, low-
level chlorine
pH, turbidity, low
pH, turbidity, low-
level chlorine
In this example the permit holder only needs to have
In this example the permit holder only needs to have a proficiency test for pH turbidity and low a proficiency test for pH turbidity and low level level a proficiency test for pH, turbidity, and low a proficiency test for pH, turbidity, and low-level level
permit, there is no need to have a proficiency. permit, there is no need to have a proficiency.
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Approved providers are found in the
Approved providers are found in the
Through the A2LA website
http://www.a2la.org/dirsearchnew/nelacptproviders.cfm
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Test as close as possible to a routine sample
Record results and report to the proficiency
Two acceptable study types Two acceptable study types Two acceptable study types
DMR
DMR-
QA – – longer time frame for completing longer time frame for completing
WP (Water Pollution)
WP (Water Pollution) – – 45 days 45 days
Providers will provide a graded result after the
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Need to have an EPA and/or AZ lab
EPA provides these free of charge by
Charles Feldmann, US EPA Charles Feldmann, US EPA 26 W Martin Luther King Drive M/S 140 26 W Martin Luther King Drive M/S 140 26 W. Martin Luther King Drive, M/S 140 26 W. Martin Luther King Drive, M/S 140 Cincinnati, OH 45268 Cincinnati, OH 45268 Tel: (513) 569 Tel: (513) 569-
7671 Fax: (513) 569 Fax: (513) 569-
7191
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E-
mail: feldmann.charles@epa.gov feldmann.charles@epa.gov
Proficiency Report Report Example
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You must contact the laboratory that
You must contact the laboratory that
Example:
Example:
Lab A – – Majority of testing for zinc, alkalinity Majority of testing for zinc, alkalinity
Lab B – Majority of testing for ammonia, nitrite Majority of testing for ammonia, nitrite
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j y g j y g
Provide contract lab with specific analyte
Provide contract lab with specific analyte
Provide date need graded results by
Provide date need graded results by
Ask contract laboratory how they will
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Arizona will allow any Water Pollution (WP)
Arizona will allow any Water Pollution (WP)
January 1st
st – Must start after this date
Must start after this date
July 2nd
nd – Must close before or on this date
Must close before or on this date
The allowed proficiency studies do not all
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Send all graded results to DMRQA
Review the information to determine if they
If unacceptable, a corrective action must be
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A review of original analysis
Another proficiency performed
A written report of steps taken
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Review should include:
Standards – expired or not expired or not
Standards – expired or not expired or not
Calibration – – meets criteria meets criteria
Quality Control Samples – meet criteria meet criteria y p y p
Maintenance of instrument/equipment used
Sample result at or near reporting level or instrument sensitivity instrument sensitivity
Analyst/Operator training
Transcription/Dilution errors
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Transcription/Dilution errors
Image from SOX First Management and Compliance Web
Another proficiency sample must be
Arizona accepts quick responses or rapid
If a study will not end until after the date listed
2010 date is Sept. 30th
th
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Once the review is completed and a new
If another unacceptable is received, contact the coordinator immediately coordinator immediately
Must send to state coordinator by deadline
Needs to provide information about what may
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http://www.epa.gov/compliance/monitoring/pr
http://www.a2la.org/dirsearchnew/nelac
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th Avenue
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