Scope Review (draft): Purity Monitors for DUNE Jianming Bian (UC - - PowerPoint PPT Presentation

scope review draft purity monitors for dune
SMART_READER_LITE
LIVE PREVIEW

Scope Review (draft): Purity Monitors for DUNE Jianming Bian (UC - - PowerPoint PPT Presentation

Scope Review (draft): Purity Monitors for DUNE Jianming Bian (UC Irvine) Andrew Renshaw (U of Houston) Stephen Pordes (Fermilab) 1 Motivation of Purity Monitors Cryostat Operation (cryostat+inline): monitor argon filling during


slide-1
SLIDE 1

Scope Review (draft): Purity Monitors for DUNE

Jianming Bian (UC Irvine) Andrew Renshaw (U of Houston) Stephen Pordes (Fermilab)

1

slide-2
SLIDE 2

Motivation of Purity Monitors

  • Cryostat Operation (cryostat+inline): monitor

argon filling during commissioning, alert pump and cryogenic accidents during

  • peration, alert unexpected contamination
  • Provide benchmarks LAr purities for

recirculation studies and TPC calibration

  • Measure e-lifetime for TPC
  • Measure purity stratification
  • Verify CDF

2

slide-3
SLIDE 3

Scope of work

  • UCI, UH and Fermilab are involved
  • Build 6 PrM in the DUNE cryostat, 4 standard and 2 long
  • Build 4 standard PrM within recirculation (inline)
  • Build electric and optical feedthroughs
  • Build two mounting structures and top flanges
  • Build FEB Electronics
  • DAQ
  • Xenon light sources with Faraday cage
  • HV and LV

3

slide-4
SLIDE 4

How was output from the purity monitors used in ProtoDUNE and for which operational phases was the data collected critical?

  • Continuously (hourly) monitor LAr Purity during filling (July23-Sep29):

Start to Monitoring purity right after bottom PrM submerged LAr, found filter saturation during the filling à report to cryo people to regenerate cartridges

  • During beam data taking (Sep – Dec 2018): Monitoring LAr Purity a few

times a day, alerted the experiment solely to serious problems several times

  • recirculation pump stoppages, false alarms, problems from the cryostat-

level gauges. prevented situations which otherwise would have continued unnoticed for some time, with severe consequences to the ability to take any data. Neither the gas analyzers nor the TPC caught these problems in time.

  • During beam and cosmic ray data taking (Sep 2018 - now): Provides

benchmark LAr purities for recirculation studies and TPC calibration, measure e-lifetime for TPC

  • Critical to LAr filling and beam data taking, critical to TPC calibration and

recirculation study

4

slide-5
SLIDE 5

Monitor LAr Purity during filling

5

As soon as the lowest purity monitor was immersed: ~40 us -> 7.5 ppb O2eq On Thursday 30st of August purity was compatible with ~60 us Cathode signal Anode signal ProtoDUNE-SP: On Friday 31st of August, 2018 the purity of the bulk liquid argon dropped from 40 us purification cartridges needed to be regenerated. Regeneration took till the 3rd of September. Filling restarted immediately after. Filippo Resnati - DUNE Collaboration Meeting - CERN - 28th January 2019

Monitor purity during LAr filling, find saturation during the filling

slide-6
SLIDE 6

Monitoring LAr Purity During Operation

6

During data taking, ProtoDUNE-SP, PrMs have alerted the experiment solely to serious problems several times (dips): Recirculation pump stoppages, false alarms, and problems from the cryostat-level gauges. These alerts are critical to the ProtoDUNE-SP project's success, as they prevented situations which otherwise would have continued unnoticed for some time, with severe consequences to the ability to take any data. Neither the gas analyzers nor the TPC caught these problems in time.

slide-7
SLIDE 7

7

slide-8
SLIDE 8

Lifetime for Cryogenic System Studies

Mar 12, 2019 8

reduced pump speed All boil-off filtered pump off All boil-off vented pump off All boil-off GAr condensed and returned Pump restart P1 P2 P3 P4 P5

Ilsoo Seong

PrMs are sensitive to purity change Typically no regular TPC data when testing recirculation

slide-9
SLIDE 9

9

slide-10
SLIDE 10

PrM vs. TPC e-lifetime

10

Bottom PrM Mean = 4.85ms RMS = 0.19 ms Mid PrM Mean = 6.20ms RMS = 0.40 ms Top PrM Mean = 6.99ms RMS = 0.36 ms TPC lifetime 2 Mean = 6.1ms RMS = 2.0 ms PrM : 200 flashes/measurement TPC lifetime 1 Mean = 4.6, 6.1ms RMS = 1.0, 1.4 ms

PrM e-lifetime stat. error is much smaller than TPC because it measures localized purity with large statistics

slide-11
SLIDE 11

Lifetime for TPC calibrate

11

Choose TPC cosmic runs under same PrM purities for e-lifetime calibration Important for DUNE because cosmic rate is low

slide-12
SLIDE 12

Lifetime for TPC calibrate

12

Electron lifetime: tau = 1/k_A*ns , where k_A is the electron attachment rate and ns is the concentration of a certain type of impurity. Attachment rates k_A at different E-fields are different, make electron lifetime and Qa/Qc different in TPC and PrM different due to their different operation HVs Develop TPC-PrM combined lifetime measurement: (Qa/Qc)_TPC= f*(Qa/Qc)_PrM f obtained from fit to (1/tau0-1/tau)_TPC vs. (1/tau0-1/tau)_PrM in data, space charge effects largely cancelled Result consistent with prediction from SCE corrected e-lifetime time prediction by Flavio and Xiao)

Craig Thorn, LBNE-Doc-4482-v1, Xin Qianhttps://indico.fnal.gov/event/14296/contributi

  • n/0
slide-13
SLIDE 13

Is the purity stratification observed within the ProtoDUNE-SP cryostat real and if so, is this consistent with initial purity measurements from cosmic rays?

  • We see hints from purity monitors, but we need to

calibrate relative difference among purity monitors to address purity stratification in ProtoDUNE-SP

  • TPC lifetime measurements affected by statistics, space

charge effects and other non-uniformity issues. E- lifetime measurements with different TPC methods are different, varying from 8 – 30ms

  • Until now ProtoDUNE-SP does not have reliable

electron lifetime from TPC, therefore, there is no purity stratification measurements from TPC

13

slide-14
SLIDE 14

Uncertainties

  • Included the run-to-run variations as a systematic error
  • Note that the table shows the relative error of each source, not the lifetime

14

τ lifetime = − tdrift log QA QC f RC

A

f RC

C

ftrans !

<latexit sha1_base64="(nul)">(nul)</latexit><latexit sha1_base64="(nul)">(nul)</latexit><latexit sha1_base64="(nul)">(nul)</latexit><latexit sha1_base64="(nul)">(nul)</latexit>

Relative uncertainties, affect sensitivity to catch purity change

0.55% in eq. Qa/Qc

slide-15
SLIDE 15

Lifetime with 1-sigma band for absolute (overall) uncertainty

15 Absolute uncertainty 5-9% in lifetime at ~7ms, dominated by transparency correction and anode/cathode gain correction Gain uncertainty can be calibrated in vacuum à Will do so when we pull PrM Assembly out to prepare for protoDUNE-SP run2 Transparency correction uncertainty can be prevented if we have longer purity monitors

Hints for e-lifetime stratification

slide-16
SLIDE 16

PrM vs. TPC e-lifetime

16

Bottom PrM Mean = 4.85ms RMS = 0.19 ms Mid PrM Mean = 6.20ms RMS = 0.40 ms Top PrM Mean = 6.99ms RMS = 0.36 ms TPC lifetime 2 Mean = 6.1ms RMS = 2.0 ms PrM : 200 flashes/measurement TPC lifetime 1 Mean = 4.6, 6.1ms RMS = 1.0, 1.4 ms

PrM e-lifetime stat. error is much smaller than TPC because it measures localized purity with large statistics

slide-17
SLIDE 17

What are the limitations of the purity monitors in terms of measuring high purity levels and what are the benefits that would be obtained by implementing proposed improvements to these devices? For Detector Operation (relative measurement):

  • Statistical Qa/Qc uncertainty < 1% à very sensitive to catch purity change

for LArTPC operation

  • To catch lifetime change at 5 sigma need Qa/Qc < (1-5*1%) = 0.95,

equivalent to 42 ms lifetime for regular PrM drift time 2.2ms For absolute lifetime measurement:

  • TODO: Draw a plot error vs. lifetime based on current absolute difference
  • TODO: To understand stratification.draw a plot of observed stratification
  • vs. error vs. purity
  • TO:DO Double the length Qa/Qc = ½(Qa/Qc)_0, draw predicted errors
  • TODO: Remove transparency correction with longer purity monitor?

17

slide-18
SLIDE 18

Lifetime with 1-sigma band for relative uncertainty

18

Uncertainty of lifetime measurement relative to each purity monitor is small Very sensitive to catch purity change caused by recirculation problems

slide-19
SLIDE 19

Lifetime with 1-sigma band for absolute (overall) uncertainty

19 Absolute uncertainty 5-9% in lifetime at ~7ms, dominated by transparency correction and anode/cathode gain correction Gain uncertainty can be calibrated in vacuum à Will do so when we pull PrM Assembly out to prepare for protoDUNE-SP run2 Transparency correction uncertainty can be prevented if we have longer purity monitors

Hints for e-lifetime stratification

slide-20
SLIDE 20

Are the proposed number of purity monitors per far detector module (10 total, 6 inside cryostat, 4 inline within cryogenic infrastructure) necessary to meet critical system requirements?

  • Two sides purity difference, understand where the

contamination from à two strings on each sides, measuring purity at different heights

  • Monitor purity right after filling à bottom PrM
  • Monitor purity closer to outgas from surface à top PrM
  • Monitor purity in the main volume of argon à middle PrM
  • Needs to measure stratification
  • à 6 PrMs in cryostat
  • Two inline purity monitors, before after LAr filtering
  • Two as replacements for the inline purity monitors
  • à 4 inline PrMs

20

slide-21
SLIDE 21

Cryostat Purity Monitors

21

One of DN250 instrumentation ports on each side, if not available then use part of manhole on each side

Need straight detector port Two strings of purity monitor assemblies on TCO and back sides, each string mounts 3 purity monitors on a supporting tube, in total 6 purity monitors in cryostat Similar system runs successfully in ProtoDUNE-SP Locations for Inline Purity monitors under discussion

slide-22
SLIDE 22

Measure purity stratification

  • Measure purity non-uniformity and help to tune CFD model (South Dakota)

22

slide-23
SLIDE 23

Inline Purity monitors

23

4 purity monitors outside of cryostat but within both in front of and behind the filtration system.

slide-24
SLIDE 24

Do the purity monitors need to be designed to operate over the full lifetime of the experiment?

  • Yes
  • Critical to all phases of detector operation
  • DUNE's large-scale FD increases the risk of failing to notice

unexpected cryogenic and circulation failures. If these conditions were to persist, it could cause irreversible contamination to the LAr and terminate useful data taking. Well scheduled PrM runs can catch sudden drops in e-lifetime, therefore mitigate this risk. PrMs' role to mitigate this risk is unique because the cosmic-ray rate in DUNE's deep-underground FD is too low for TPC to measure e- lifetime frequently with its data.

  • Provide benchmarks LAr purities for recirculation studies and TPC

calibration

  • Measure e-lifetime for TPC
  • Measure purity stratification
  • Verify CDF

24

slide-25
SLIDE 25

Are the proposed mechanisms for supporting the monitors within the cryostat and connecting them to the outside of cryostat mechanically sound and cost effective?

  • According to ProtoDUNE-SP, the supporting

macnism is robust, supporting structure cost is ~$10k (discuss why need straight port and why can’t use cable tray?)

  • ProtoDUNE-SP doesn’t have inline purity
  • monitors. DUNE inline PrM supporting structures

will follow 35t and LAPD inline purity monitors. The major cost of inline purity monitor supporting is the cost of vessles that contain purity monitors, $100k/each at CERN

25

slide-26
SLIDE 26

Backup

26

slide-27
SLIDE 27

27

Successfully run at ProtoDUNE-PS, find saturation, alert pump stoppage, pump recirculation, measure e-lifetime combined with TPC

slide-28
SLIDE 28

ProtoDUNE-SP Purity Monitors

Top PrM Middle PrM Bottom PrM Individual PrMon:

  • Xe flash lamp light source
  • Al-Ti-Au photocathode for drift

electron generation

  • Cathode/anode gates for charge

screening at readout

  • Internal cable shields tied to

PrMon cage and flange

  • M. Adamowski et al., JINST 9, P07005 (2014).

Qanode/Qcathode = e-tdrift/t

28

Clean LAr Distribution Dirty LAr pump

slide-29
SLIDE 29

Improved on purity monitor signal

29

  • HV variation (0.25kV-3kV) + transparency correction

making electron drift time range from 150 us to 3 ms.

  • Used 8 fibers to deliver UV light for each purity monitor

Signals on anode and cathode are 6 times larger.

  • Allows PrMs measuring e-lifetime 35us - 10ms with high

precision.

  • At 6 ms (purity for most of H4 beam time), Qa/Qc = 0.7 à

no saturation ProtoDUNE PrM signals at e-lifetime = 6 ms

slide-30
SLIDE 30

Lifetime with 1-sigma band for relative uncertainty

30

Uncertainty of lifetime measurement relative to each purity monitor is small Very sensitive to catch purity change caused by recirculation problems

slide-31
SLIDE 31

Electronics

04/26/17 ProtoDUNE-SP Cryogenics Instrumentation Review 31

Fermilab Particle Physics Division Site Support Department S i z e FSCH No DWG No R e v S c a l e S h e e t Issued Originated: Last Revision: Drawn by: T i t l e B Originator: P r o j e c t Gerard Visser Walter Jaskierny 30 Aug 2004

Purity Monitor Electronics Type 2, Two Channel

FLARE 1 of 2 GND 750 pf 15 KV 10 M Ω 10 M Ω 10 M Ω 50 M Ω 750 pf 15 KV 7 3 9, 5 1 2,4 6,8 DZero Preamp 5 pf 20 Meg 16 Aug 2007 Amp 1 Anode SHV Negative Cathode Supply 2kV Max. 100 M Ω 499 Ω *See Notes LM317 7906 249 Ω 1N458 1.33 KΩ 22 µf 15 WVDC 0.1 µf 0.1 µf 0.1 µf 0.1 µf 1N4002 1N4002 0.1 µf 0.1 µf +12 V
  • 12 V
COM +8 V
  • 6 V
220 µf 10 V 220 µf 10 V SHV SHV SHV SHV To Anode To Anode Grid To Cathode Positive Anode Supply 10kV Max. **See Notes Amp 1 Test Pulse LEMO Amp 1 Output 100 Ω 5 W Sig Gnd Notes: * Reduce this resistor value for lower noise but less protection
  • f amplifier. This resistor effects both gain and low frequency roll off.
** SHV connectors limit upper voltage to 5 kV unterminated, 7.5 kV terminated. *** Components matched in 1% pairs External LV DC supply should be floating to avoid 60 Hz pickup. Mount all HV components rigidly. Electrotatic shielding and corona dope required for lower noise. TP3 1000:1 100 K Ω 1000 pf 1 kV TP5 TP4 1 KΩ 1 KΩ GND Ckt Com 1 6 1 7 3 4 49.9 Ω 2 pf Amp 2 Test Pulse LEMO 500 MΩ 49.9 Ω 2 pf EC75X +8V
  • 6V
Amp 1 Cathode Sig Gnd Amp 2 Anode Sig Gnd Amp 2 Cathode Sig Gnd GND 7 3 9, 5 1 2,4 6,8 DZero Preamp 5 pf 20 Meg 499 Ω *See Notes 0.1 µf 0.1 µf Amp 2 Output LEMO A1-1 A1-2 C1-1 C1-2 A2-1 A2-2 C2-1 C2-2 LEMO T = 1 e-4 Sec. T = 1 e-4 Sec. 500 MΩ EC75X 0.01µf 3KV 0.01µf 3KV 0.01µf 3KV 0.01µf 3KV 1000 pf 1 kV 1500 M Ω SHV Anode Grid Supply 10kV Max. **See Notes 1000 pf 1 kV SHV TP2 10,000:1 TP1 10,000:1 150 K 150 K 1500 M Ω 10 M Ω 100 M Ω 15 M Ω 10 M Ω 10 M Ω 10 M Ω 50 M Ω 10 M Ω 1000pf 15KV 1000pf 15KV 1000pf 15KV 1000pf 15KV 1000pf 15KV Jumper to Anode Grid 1000pf 15KV 1000pf 15KV 0.01 µf
  • cerm. disc
Common Mode Inductor ≈325 µH Common Mode Inductor ≈325 µH Amplifiers matched to 1% for Gain and Time Constant Common Mode Inductor ≈35 µH +8V
  • 6V
Common Mode Inductor ≈35 µH C.M.L ≈10 µH C.M.L ≈10 µH F 3AG 1/2 Amp 3AG 1/2 Amp
slide-32
SLIDE 32

Flange

4X 2-3/4 CF Flanges (3-HV and signal) (1-Fiber optics) 2X 1/5” VCR (For gas fill and relief) 1X 1.33” CF Flange (Vacuum pumping) Custom support tube adapter, holes for HV cables to be inserted Side view

3XOptical feedthroughs HV feedthroughs

slide-33
SLIDE 33

HV and optical Feedthroughs

HV Feedthroughs: ~ 10kV Optical Feedthroughs:

slide-34
SLIDE 34

Flange and Mounting Parts Fabrication and Assembly

  • The overall system design is now in place,

fabrication of the parts will being immediately, flange will be first

  • Fibers will be contained within support tube,

so no worry about breakage from installation

  • Cables will be tied to the supporting tube

Flange will have support tube adapter Support tube will also contain 0.5” tube to contain fibers Hole in adapter for HV cables to enter support tube

slide-35
SLIDE 35

HV and Slow control

  • Programmable HV
  • Relay board for NIM bin (PrM electronics)
  • Relay board for DC power supply for the light source/or Programmable DC

power supply for the light source.

35

slide-36
SLIDE 36

Light source

  • Hamamatsu Xenon source (1J/flash)
  • Faraday cage for grounding

36

slide-37
SLIDE 37

PrM electronics Signal: 2 channels – cathode, anode < 5V PrM HV Cathod -150V Anode 2500V DAQ PC 110V Digitizers NIM Bin 110 V

DAQ

Need to Develop slow control

37

slide-38
SLIDE 38

Trigger

  • Photo Diode to trigger the

digitizer

  • Trigger signal also to

TPC/PDS DAQ to prevent possible noise from purity monitor

38

To TPC/PDS DAQ

slide-39
SLIDE 39

DP purity monitors

39

slide-40
SLIDE 40

Rely to important question

"Why measure with purity monitors and not in TPC data”

  • DUNE's large-scale FD increases the risk of failing to notice unexpected cryogenic and circulation failures. If these

conditions were to persist, it could cause irreversible contamination to the LAr and terminate useful data

  • taking. Well scheduled PrM runs can catch sudden drops in e-lifetime, therefore mitigate this risk. PrMs' role to

mitigate this risk is unique because the cosmic-ray rate in DUNE's deep-underground FD is too low for TPC to measure e-lifetime frequently with its data.

  • At ProtoDUNE where we have enough TPC cosmic ray data to measure electron lifetime online, the large

fluctuation in the online e-lifetime from TPC data makes it hard to catch the purity change caused by liquid argon recirculation issue in time. On the other hand, after lower the purity monitor anode high voltage, electron drift time in purity monitors reaches 2.2 ms, the same as the TPC, but the purity monitor can take large statistics in a short period of time at the same location, so the statical error and effects from location dependent uncertainties are smaller in purity monitors compared with TPC. Each purity monitor e-lifetime measurement is based on purity monitor Qa/Qc from 200 UV flashes within 40 seconds at the same location, and the statistic error on the purity monitor e-lifetime is less than 0.03 ms when the purity is 6 ms. With this high precision, purity monitors can catch the purity drop immediately and make the alert to the experiment.

  • During the commissioning and operation of ProtoDUNE-SP, PrMs have alerted the experiment solely to serious

problems several times. The first time was for filter saturation during LAr filling, and the rest were recirculation pump stoppages, false alarms, and problems from the cryostat-level gauges. These alerts are crucial to the ProtoDUNE-SP project's success, as they prevented situations which otherwise would have continued unnoticed for some time, with severe consequences to the ability to take any data. Neither the gas analyzers nor the TPC caught these problems in time.

40

slide-41
SLIDE 41

Test PrMs in long tube

  • After assemble PrMs on long supporting rods, test the full

assembly in vacuum

SS tube Stephen, Filippo

slide-42
SLIDE 42
  • After assemble PrMs on long supporting rods, check

electric/optical connections

  • Move the PrM assembly to the corridor
  • Use crane, lift and rotate the assembly 90 degrees
  • Use crane, move the assembly to the top of the port
  • Use crane, start to insert the assembly into the port
  • Test connections on each PrM vertically during insertion
  • After insertion, test overall resistance and capacitance with

electrometer and Capacitance Meter meter

  • Mount NIM bin and Xe flash lamp on the PrM.
  • Connect cables
  • Connect optical fibers to Xe flash lamp
  • Make connections to power supplies and slow controls

interfaces

Installation procedure

slide-43
SLIDE 43

Check connections one by one during insertion

Crane Port Use multimeter to test connectivity to feedthrough/topflange for cathode, anode, anode grid and ground with faraday cage Insert slowly, stop when checking connections If fibers are not closely attached to the cathode surface, open the side window of the Farady cage and tune Testing cables x 9 UCI sling <150 lbs